SYNTHESIS, SPECTROSCOPIC CHARACTERIZATION, X-RAY CRYSTAL STRUCTURE, BIOLOGICAL SCREENING AND CATALYTIC STUDIES OF ORGANOTIN (IV) CARBOXYLATES OF 3-(4-CYANOPHENYL) ACRYLIC ACID

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TARIQ MUHAMMAD; ALI SAQIB; TAHIR MUHAMMAD NAWAZ; KHALID NASIR; SHIRAZI JAFIR HUSSAIN

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Journal: JOURNAL OF THE IRANIAN CHEMICAL SOCIETY(JICS) Year:2014 | Volume:11 | Issue:3 Page(s): 839-846

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Title

SYNTHESIS, SPECTROSCOPIC CHARACTERIZATION, X-RAY CRYSTAL STRUCTURE, BIOLOGICAL SCREENING AND CATALYTIC STUDIES OF ORGANOTIN (IV) CARBOXYLATES OF 3-(4-CYANOPHENYL) ACRYLIC ACID

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Keywords

ORGANOTIN (IV) CARBOXYLATE

ANTIMICROBIAL ACTIVITY

TRANSESTERIFICATION

BIODIESEL

Abstract

A series of six organotin (IV) carboxylates [Me2SnL2] (1), [n-Bu2SnL2] (2), [n-Oct2SnL2] (3), [Me3SnL] (4), n-Bu3SnL (5) and [Ph3SnL] (6), where L = 3-(4-cyanophenyl) acrylic acid have been synthesized and characterized by elemental analysis, FT-IR and NMR (1H, 13C). The complex (4) was also analyzed by single crystal X-ray analysis which showed distorted trigonal bipyramidal geometry with polymeric bridging behavior. The complexes 1–6 were screened for antimicrobial activities and cytotoxicity. The results showed significant activity with few exceptions. The catalytic activity of complexes was assessed in TRANSESTERIFICATION reaction of Brassica campestris oil (triglycerides) to produce BIODIESEL (fatty acid methyl esters). The results showed that triorganotin (IV) complexes exhibited good catalytic activity than their di-analogues.

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APA: Copy

TARIQ, MUHAMMAD, ALI, SAQIB, TAHIR, MUHAMMAD NAWAZ, KHALID, NASIR, & SHIRAZI, JAFIR HUSSAIN. (2014). SYNTHESIS, SPECTROSCOPIC CHARACTERIZATION, X-RAY CRYSTAL STRUCTURE, BIOLOGICAL SCREENING AND CATALYTIC STUDIES OF ORGANOTIN (IV) CARBOXYLATES OF 3-(4-CYANOPHENYL) ACRYLIC ACID. JOURNAL OF THE IRANIAN CHEMICAL SOCIETY(JICS), 11(3), 839-846. SID. https://sid.ir/paper/282759/en

Vancouver: Copy

TARIQ MUHAMMAD, ALI SAQIB, TAHIR MUHAMMAD NAWAZ, KHALID NASIR, SHIRAZI JAFIR HUSSAIN. SYNTHESIS, SPECTROSCOPIC CHARACTERIZATION, X-RAY CRYSTAL STRUCTURE, BIOLOGICAL SCREENING AND CATALYTIC STUDIES OF ORGANOTIN (IV) CARBOXYLATES OF 3-(4-CYANOPHENYL) ACRYLIC ACID. JOURNAL OF THE IRANIAN CHEMICAL SOCIETY(JICS)[Internet]. 2014;11(3):839-846. Available from: https://sid.ir/paper/282759/en

IEEE: Copy

MUHAMMAD TARIQ, SAQIB ALI, MUHAMMAD NAWAZ TAHIR, NASIR KHALID, and JAFIR HUSSAIN SHIRAZI, “SYNTHESIS, SPECTROSCOPIC CHARACTERIZATION, X-RAY CRYSTAL STRUCTURE, BIOLOGICAL SCREENING AND CATALYTIC STUDIES OF ORGANOTIN (IV) CARBOXYLATES OF 3-(4-CYANOPHENYL) ACRYLIC ACID,” JOURNAL OF THE IRANIAN CHEMICAL SOCIETY(JICS), vol. 11, no. 3, pp. 839–846, 2014, [Online]. Available: https://sid.ir/paper/282759/en

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