AN EFFICIENT ROUTE TO BICYCLE [3.3.1] INTERMEDIATE EMPLOYING ORGANOCATALYTIC MICHAEL/ALDOL BIANNULATION: A FORMAL SYNTHESIS OF (+)-HUPERZINE A

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ZHANG CHAO; HE YU PENG; LV ZHENBO; DING XIAOGUANG; LI FEI; YU FANG

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ISSN: 2588-4824

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Journal: JOURNAL OF THE IRANIAN CHEMICAL SOCIETY(JICS) Year:2016 | Volume:13 | Issue:8 Page(s): 0-0

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Title

AN EFFICIENT ROUTE TO BICYCLE [3.3.1] INTERMEDIATE EMPLOYING ORGANOCATALYTIC MICHAEL/ALDOL BIANNULATION: A FORMAL SYNTHESIS OF (+)-HUPERZINE A

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Keywords

(+)-HUPERZINE AORGANO CATALYST ENANTIO SELECTIVITY MICHAEL ADDITION

Abstract

The key intermediate for the synthesis of (+)-Huperzine A, bicycle[3.3.1]nona-2,6-dien-9-one core, was prepared by Michael–Aldol annulation of b-ketoesters and methacrolein catalyzed by a, a-diarylprolinol silyl ether in highest 87 % ee and with up to 80 % ee in the gram-scale procedure.

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APA: Copy

ZHANG, CHAO, HE, YU PENG, LV, ZHENBO, DING, XIAOGUANG, LI, FEI, & YU, FANG. (2016). AN EFFICIENT ROUTE TO BICYCLE [3.3.1] INTERMEDIATE EMPLOYING ORGANOCATALYTIC MICHAEL/ALDOL BIANNULATION: A FORMAL SYNTHESIS OF (+)-HUPERZINE A. JOURNAL OF THE IRANIAN CHEMICAL SOCIETY(JICS), 13(8), 0-0. SID. https://sid.ir/paper/283200/en

Vancouver: Copy

ZHANG CHAO, HE YU PENG, LV ZHENBO, DING XIAOGUANG, LI FEI, YU FANG. AN EFFICIENT ROUTE TO BICYCLE [3.3.1] INTERMEDIATE EMPLOYING ORGANOCATALYTIC MICHAEL/ALDOL BIANNULATION: A FORMAL SYNTHESIS OF (+)-HUPERZINE A. JOURNAL OF THE IRANIAN CHEMICAL SOCIETY(JICS)[Internet]. 2016;13(8):0-0. Available from: https://sid.ir/paper/283200/en

IEEE: Copy

CHAO ZHANG, YU PENG HE, ZHENBO LV, XIAOGUANG DING, FEI LI, and FANG YU, “AN EFFICIENT ROUTE TO BICYCLE [3.3.1] INTERMEDIATE EMPLOYING ORGANOCATALYTIC MICHAEL/ALDOL BIANNULATION: A FORMAL SYNTHESIS OF (+)-HUPERZINE A,” JOURNAL OF THE IRANIAN CHEMICAL SOCIETY(JICS), vol. 13, no. 8, pp. 0–0, 2016, [Online]. Available: https://sid.ir/paper/283200/en

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