SYNTHESIS, CHARACTERIZATION, SPECTROSCOPIC AND CATALYTIC OXIDATION STUDIES OF FE(III), NI(II), CO(III), V(IV) AND U(VI) SCHIFF BASE COMPLEXES WITH N, O DONOR LIGANDS DERIVED FROM 2, 3-DIAMINOPYRIDINE

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ZABARDASTI ABEDIEN; SHANGAIE SAYED ASAD

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Journal: JOURNAL OF THE IRANIAN CHEMICAL SOCIETY(JICS) Year:2016 | Volume:13 | Issue:10 Page(s): 0-0

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Title

SYNTHESIS, CHARACTERIZATION, SPECTROSCOPIC AND CATALYTIC OXIDATION STUDIES OF FE(III), NI(II), CO(III), V(IV) AND U(VI) SCHIFF BASE COMPLEXES WITH N, O DONOR LIGANDS DERIVED FROM 2, 3-DIAMINOPYRIDINE

Author(s)

ZABARDASTI ABEDIEN | SHANGAIE SAYED ASAD | Issue Writer Certificate

Keywords

SCHIFF BASE2

3-DIAMINOPYRIDINEX-RAY

CRYSTALLOGRAPHY CATALYTIC

EPOXIDATION STYRENE TRANSITION METAL

IONS

Abstract

Fifteen new complexes of transition metals were designed using three Schiff base ligands and aldol condensation of 2, 3-diaminopyridine with 5-R-2-hydroxybenzaldehyde (R = F, Cl, Br) in the 1:2 molar ratio. The tetradentate ligands N, N’-bis (5-R-2-hydroxybenzaldehyde) pyridine were acquired with the common formula H2 [(5-R-sal) 2py] and characterized by IR, UV–Vis spectra, 1H-NMR and elemental analysis. These ligands produce 1:1 complexes M [(5-R-sal) 2py] with Fe (III), Ni(II), Co(III), V(IV) and U(VI) metal IONS. The electronic property and nature of complexes were identified by IR, UV–Vis spectra, elemental analysis, X-ray crystallography and cyclic voltammetric methods. The catalytic activity of complexes for epoxidation of styrene with UHP as primary oxidant at minimal temperature (10oC) has been planned. The spectral data of the ligands and their complexes are deliberate in connection with the structural changes which happen due to complex preparation. The electrochemical outcome has good conformability with what suggested for electronic interaction among metal center and ligand by the UV–Vis and IR measurements.

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APA: Copy

ZABARDASTI, ABEDIEN, & SHANGAIE, SAYED ASAD. (2016). SYNTHESIS, CHARACTERIZATION, SPECTROSCOPIC AND CATALYTIC OXIDATION STUDIES OF FE(III), NI(II), CO(III), V(IV) AND U(VI) SCHIFF BASE COMPLEXES WITH N, O DONOR LIGANDS DERIVED FROM 2, 3-DIAMINOPYRIDINE. JOURNAL OF THE IRANIAN CHEMICAL SOCIETY(JICS), 13(10), 0-0. SID. https://sid.ir/paper/283246/en

Vancouver: Copy

ZABARDASTI ABEDIEN, SHANGAIE SAYED ASAD. SYNTHESIS, CHARACTERIZATION, SPECTROSCOPIC AND CATALYTIC OXIDATION STUDIES OF FE(III), NI(II), CO(III), V(IV) AND U(VI) SCHIFF BASE COMPLEXES WITH N, O DONOR LIGANDS DERIVED FROM 2, 3-DIAMINOPYRIDINE. JOURNAL OF THE IRANIAN CHEMICAL SOCIETY(JICS)[Internet]. 2016;13(10):0-0. Available from: https://sid.ir/paper/283246/en

IEEE: Copy

ABEDIEN ZABARDASTI, and SAYED ASAD SHANGAIE, “SYNTHESIS, CHARACTERIZATION, SPECTROSCOPIC AND CATALYTIC OXIDATION STUDIES OF FE(III), NI(II), CO(III), V(IV) AND U(VI) SCHIFF BASE COMPLEXES WITH N, O DONOR LIGANDS DERIVED FROM 2, 3-DIAMINOPYRIDINE,” JOURNAL OF THE IRANIAN CHEMICAL SOCIETY(JICS), vol. 13, no. 10, pp. 0–0, 2016, [Online]. Available: https://sid.ir/paper/283246/en

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