مرکز اطلاعات علمی Scientific Information Database (SID) - Trusted Source for Research and Academic Resources

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Information Journal Paper

Title

ROOM TEMPERATURE AQUEOUS PHASE SYNTHESIS AND CHARACTERIZATION OF NOVEL NANO-SIZED COORDINATION POLYMERS COMPOSED OF COPPER (II), NICKEL (II), AND ZINC (II) METAL IONS WITH P-PHENYLENEDIAMINE (PPD) AS THE BRIDGING LIGAND

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Abstract

 NANOSTRUCTURED metal-organic hybrid materials composed of nickel (II), copper (II), and zinc (II) metal ions and P-PHENYLENEDIAMINE (PPD) as the organic ligand were synthesized in AQUEOUS MEDIUM at room temperature. The synthesized compounds were characterized by elemental analyses, powder X-ray diffraction (PXRD) spectra, Fourier transform infrared spectra, nuclear magnetic resonance (1H NMR) spectra, electronic spectra, scanning electron microscopy, N2 adsorption-desorption isotherm, and dynamic light scattering studies. N2 adsorption-desorption isotherm of copper (II) -PPD compound confirmed that it has MESOPOROUS structure as it exhibits type-IV reversible isotherm with H1 hysterisis. Steep adsorption indicated that the mesopores possessing it are of uniform order. Barrett-Joyner- Halenda model showed an average pore diameter of 5.2 nm. The PXRD patterns of all the three compounds are identical and showed well-defined and highly intense diffraction peaks, thereby suggesting their nature as CRYSTALLINE. The broadness of the diffraction peaks indicated that the particles are of nanometer dimensions.

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    APA: Copy

    GUPTA, RIMPY, SANOTRA, SUMIT, SHEIKH, HAQ NAWAZ, & KALSOTRA, BANSI LAL. (2013). ROOM TEMPERATURE AQUEOUS PHASE SYNTHESIS AND CHARACTERIZATION OF NOVEL NANO-SIZED COORDINATION POLYMERS COMPOSED OF COPPER (II), NICKEL (II), AND ZINC (II) METAL IONS WITH P-PHENYLENEDIAMINE (PPD) AS THE BRIDGING LIGAND. JOURNAL OF NANOSTRUCTURE IN CHEMISTRY, 3(3), 0-0. SID. https://sid.ir/paper/333146/en

    Vancouver: Copy

    GUPTA RIMPY, SANOTRA SUMIT, SHEIKH HAQ NAWAZ, KALSOTRA BANSI LAL. ROOM TEMPERATURE AQUEOUS PHASE SYNTHESIS AND CHARACTERIZATION OF NOVEL NANO-SIZED COORDINATION POLYMERS COMPOSED OF COPPER (II), NICKEL (II), AND ZINC (II) METAL IONS WITH P-PHENYLENEDIAMINE (PPD) AS THE BRIDGING LIGAND. JOURNAL OF NANOSTRUCTURE IN CHEMISTRY[Internet]. 2013;3(3):0-0. Available from: https://sid.ir/paper/333146/en

    IEEE: Copy

    RIMPY GUPTA, SUMIT SANOTRA, HAQ NAWAZ SHEIKH, and BANSI LAL KALSOTRA, “ROOM TEMPERATURE AQUEOUS PHASE SYNTHESIS AND CHARACTERIZATION OF NOVEL NANO-SIZED COORDINATION POLYMERS COMPOSED OF COPPER (II), NICKEL (II), AND ZINC (II) METAL IONS WITH P-PHENYLENEDIAMINE (PPD) AS THE BRIDGING LIGAND,” JOURNAL OF NANOSTRUCTURE IN CHEMISTRY, vol. 3, no. 3, pp. 0–0, 2013, [Online]. Available: https://sid.ir/paper/333146/en

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