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Information Journal Paper

Title

Electrochemical activity of Ni‑ montmorillonite/Vulcan XC‑ 72R carbon black nano‑ catalyst for the oxidation of methanol in acidic medium

Author(s)

 Sheikh Mohseni Mohammad Hossein | SEDAGHAT SAJJAD | DERAKHSHI PIROUZ | SAFEKORDI ALIAKBAR | Issue Writer Certificate 

Pages

  217-224

Abstract

 Direct methanol fuel cell is claiming to be the most main power source in future as a clean energy source, for which methanol is used as fuel. In the present study, nickel nanoparticles were synthesized by green route in the presence of montmorillonite (Ni-MMT). Then the electrochemical activity of prepared nanocomposite was investigated in methanol oxidation reaction in acidic medium. In the process of nickel nanoparticle synthesis, the natural substrate montmorillonite was used as capping agent and Allium jesdianum water extract was used as the source of reducing agent for the first time. The Ni-MMT sample was characterized by UV– Vis, XRD, SEM and EDX techniques. Production of nickel nanoparticles in the proposed green method is confirmed by absorption peak of 405 nm in UV– Vis spectrum. The average particle size of Ni-MMT was determined as 20. 80 nm. The oxidation of methanol in acidic medium was studied by cyclic voltammetry using Ni-MMTmodified carbon paste electrode (Ni-MMT/CPE). Methanol was oxidized on the Modified electrode surface at 0. 3 V. Also, the catalytic current of methanol oxidation was 3 mA in H2SO4 electrolyte which is significantly more than unmodified CPE. The concentration of 0. 5 M for H2SO4 was obtained as the optimum electrolyte for the oxidation of methanol. Methanol can be catalyzed in the concentration range of 0. 1– 0. 5 M by the prepared nanostructured catalyst.

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    APA: Copy

    Sheikh Mohseni, Mohammad Hossein, SEDAGHAT, SAJJAD, DERAKHSHI, PIROUZ, & SAFEKORDI, ALIAKBAR. (2019). Electrochemical activity of Ni‑ montmorillonite/Vulcan XC‑ 72R carbon black nano‑ catalyst for the oxidation of methanol in acidic medium. JOURNAL OF NANOSTRUCTURE IN CHEMISTRY, 9(3), 217-224. SID. https://sid.ir/paper/333382/en

    Vancouver: Copy

    Sheikh Mohseni Mohammad Hossein, SEDAGHAT SAJJAD, DERAKHSHI PIROUZ, SAFEKORDI ALIAKBAR. Electrochemical activity of Ni‑ montmorillonite/Vulcan XC‑ 72R carbon black nano‑ catalyst for the oxidation of methanol in acidic medium. JOURNAL OF NANOSTRUCTURE IN CHEMISTRY[Internet]. 2019;9(3):217-224. Available from: https://sid.ir/paper/333382/en

    IEEE: Copy

    Mohammad Hossein Sheikh Mohseni, SAJJAD SEDAGHAT, PIROUZ DERAKHSHI, and ALIAKBAR SAFEKORDI, “Electrochemical activity of Ni‑ montmorillonite/Vulcan XC‑ 72R carbon black nano‑ catalyst for the oxidation of methanol in acidic medium,” JOURNAL OF NANOSTRUCTURE IN CHEMISTRY, vol. 9, no. 3, pp. 217–224, 2019, [Online]. Available: https://sid.ir/paper/333382/en

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