Investigation of intermolecular interactions in the crystal structure of 1-phenyl-1, 2-ethanediol

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bikas Rahman; emami marziesadat; Kozakiewicz Anna

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ISSN: 2588-4824

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Journal: Iranian Journal of Crystallography and Mineralogy Year:2020 | Volume:27 | Issue:4 Page(s): 959-966

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Title

Investigation of intermolecular interactions in the crystal structure of 1-phenyl-1, 2-ethanediol

Author(s)

bikas Rahman | emami marziesadat | Kozakiewicz Anna | Issue Writer Certificate

Keywords

1-Phenyl-1Q3

2-ethanediolQ1

crystal structureQ1

hydrogen bondingQ1

Abstract

1-Phenyl-1, 2-ethanediol was synthesized from the hydrolysis of epoxy styrene in water medium. The compound was characterized by FT-IR and NMR spectroscopic methods and structure was characterized by single crystal X-ray diffraction method. The crystallographic information was collected at 293 K. This compound is crystallized in the triclinic space group with unit cell parameters of a = 6. 0274(10) Å , b = 16. 204(2) Å , c = 17. 345(2) Å ; α = 117. 584(14)° , β = 99. 322(13)° , γ = 90. 047 (14)° , V = 1476. 1 (4) Å 3 and Z = 8. The asymmetric unit of the crystal structure consists of four molecules of 1-Phenyl-1, 2-ethanediol which are connected to each other by strong hydrogen bond and C-H∙ ∙ ∙ π interactions. A supramolecular network is generated by intermolecular O-H∙ ∙ ∙ O and C-H∙ ∙ ∙ O hydrogen bond interactions.

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APA: Copy

bikas, Rahman, emami, marziesadat, & Kozakiewicz, Anna. (2020). Investigation of intermolecular interactions in the crystal structure of 1-phenyl-1, 2-ethanediol. IRANIAN JOURNAL OF CRYSTALLOGRAPHY AND MINERALOGY, 27(4 ), 959-966. SID. https://sid.ir/paper/357500/en

Vancouver: Copy

bikas Rahman, emami marziesadat, Kozakiewicz Anna. Investigation of intermolecular interactions in the crystal structure of 1-phenyl-1, 2-ethanediol. IRANIAN JOURNAL OF CRYSTALLOGRAPHY AND MINERALOGY[Internet]. 2020;27(4 ):959-966. Available from: https://sid.ir/paper/357500/en

IEEE: Copy

Rahman bikas, marziesadat emami, and Anna Kozakiewicz, “Investigation of intermolecular interactions in the crystal structure of 1-phenyl-1, 2-ethanediol,” IRANIAN JOURNAL OF CRYSTALLOGRAPHY AND MINERALOGY, vol. 27, no. 4 , pp. 959–966, 2020, [Online]. Available: https://sid.ir/paper/357500/en

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