High Yield, One-Pot and Facile Synthesis of New Isobenzofuran-1(3H)-one Derivatives via Oxidation of 3a, 8a-Dihydroxyindeno[1, 2-d]imidazole-8(3H)-ones

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Mohammadi Nasim; Mohamadizadeh Mohammad Reza; SABERI DARIUSH; ABBASI MOHAMMAD

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Journal: Applied Chemistry Today Year:2018 | Volume:13 | Issue:46 Page(s): 57-66

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Title

High Yield, One-Pot and Facile Synthesis of New Isobenzofuran-1(3H)-one Derivatives via Oxidation of 3a, 8a-Dihydroxyindeno[1, 2-d]imidazole-8(3H)-ones

Author(s)

Mohammadi Nasim | Mohamadizadeh Mohammad Reza | SABERI DARIUSH | ABBASI MOHAMMAD | Issue Writer Certificate

Keywords

Trichloroacetonitrile Amines Ninhydrin IsobenzofuranQ1

1(3H)Q1

one 3aQ1

8aQ1

Dihydroxyindeno[1Q1

2Q1

d]imidazoleQ1

Abstract

Substituted isobenzofuran-1(3H)-ones and imidzoles are useful building blocks in organic synthesis due to their structural importance, chemical stability and relative accessibility. Furthermore, such structures are of important and biologically active heterocycles and they are widely present in many bioactive compounds and synthetic drugs. In this paper, a novel, one-pot and efficient procedure are introduced for the preparation of some new derivative of these compounds. At first, some of 3a, 8a-dihydroxyindeno[1, 2-d]imidazole-8(3H)-one derivatives were synthesized from the reaction of trichloroacetonitrile, amines and ninhydrin in ethanol. Then their corresponding isobenzofuran-1(3H)-ones were prepared by the one-pot oxidation of the synthesized diols using lead tetraacetate in acetic acid. Reaction well worked for various amine derivatives and final products were characterized using their IR, 1H-NMR and 13C-NMR spectra.

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APA: Copy

Mohammadi, Nasim, Mohamadizadeh, Mohammad Reza, SABERI, DARIUSH, & ABBASI, MOHAMMAD. (2018). High Yield, One-Pot and Facile Synthesis of New Isobenzofuran-1(3H)-one Derivatives via Oxidation of 3a, 8a-Dihydroxyindeno[1, 2-d]imidazole-8(3H)-ones. JOURNAL OF APPLIED CHEMISTRY, 13(46 ), 57-66. SID. https://sid.ir/paper/384704/en

Vancouver: Copy

Mohammadi Nasim, Mohamadizadeh Mohammad Reza, SABERI DARIUSH, ABBASI MOHAMMAD. High Yield, One-Pot and Facile Synthesis of New Isobenzofuran-1(3H)-one Derivatives via Oxidation of 3a, 8a-Dihydroxyindeno[1, 2-d]imidazole-8(3H)-ones. JOURNAL OF APPLIED CHEMISTRY[Internet]. 2018;13(46 ):57-66. Available from: https://sid.ir/paper/384704/en

IEEE: Copy

Nasim Mohammadi, Mohammad Reza Mohamadizadeh, DARIUSH SABERI, and MOHAMMAD ABBASI, “High Yield, One-Pot and Facile Synthesis of New Isobenzofuran-1(3H)-one Derivatives via Oxidation of 3a, 8a-Dihydroxyindeno[1, 2-d]imidazole-8(3H)-ones,” JOURNAL OF APPLIED CHEMISTRY, vol. 13, no. 46 , pp. 57–66, 2018, [Online]. Available: https://sid.ir/paper/384704/en

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