Spark Plasma Sintering of ZrB2-SiC-ZrC Nanocomposite Synthesized by MASPS

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Emami Seyed Mohsen; SALAHI ESMAEIL; ZAKERI MOHAMMAD; TAYEBIFARD SEYED ALI

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Journal: Journal of Advanced Processes in Materials Engineering Year:2020 | Volume:14 | Issue:2 Page(s): 1-11

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Title

Spark Plasma Sintering of ZrB2-SiC-ZrC Nanocomposite Synthesized by MASPS

Author(s)

Emami Seyed Mohsen | SALAHI ESMAEIL | ZAKERI MOHAMMAD | TAYEBIFARD SEYED ALI | Issue Writer Certificate

Keywords

Zirconium Diboride (ZrB2)Q1

Silicon Carbide (SiC)Q2

Zirconium Carbide (ZrC)Q1

Spark Plasma Sintering (SPS)Q1

Nano compositeQ2

Abstract

ZrB2– SiC– ZrC nanocomposite was fabricated by spark plasma sintering using ZrB2– SiC– ZrC synthesized powder by MA-SPS route. In the present research, sintering mechanism was investigated by displacement-temperature-time (DTT), displacement rate vs. temperature and displacement rate vs. time diagrams which were obtained during spark plasma sintering cycles. Sintering process of the composite was completed after 17 min at temperature of 1750° C. By using X-ray powder diffraction (XRD) pattern and Rietveld method, the mean crystallites sizes of about 77, 62 and 56 nm were calculated for ZrB2, SiC and ZrC phases, respectively. The physical and mechanical properties of sintered composite such as: density, tensile strength, Vickers hardness and fracture toughness were% 99/3, 563 MPa, 18 GPa and 4. 9 MPa. m1/2, respectively. Finally scanning electron microscopy (SEM) images show three different phases well distributed all over the sample. It is clear that ZrB2, SiC and ZrC phases are well connected and have good continuity.

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APA: Copy

Emami, Seyed Mohsen, SALAHI, ESMAEIL, ZAKERI, MOHAMMAD, & TAYEBIFARD, SEYED ALI. (2020). Spark Plasma Sintering of ZrB2-SiC-ZrC Nanocomposite Synthesized by MASPS. ADVANCED PROCESSES IN MATERIALS, 14(2 ), 1-11. SID. https://sid.ir/paper/407844/en

Vancouver: Copy

Emami Seyed Mohsen, SALAHI ESMAEIL, ZAKERI MOHAMMAD, TAYEBIFARD SEYED ALI. Spark Plasma Sintering of ZrB2-SiC-ZrC Nanocomposite Synthesized by MASPS. ADVANCED PROCESSES IN MATERIALS[Internet]. 2020;14(2 ):1-11. Available from: https://sid.ir/paper/407844/en

IEEE: Copy

Seyed Mohsen Emami, ESMAEIL SALAHI, MOHAMMAD ZAKERI, and SEYED ALI TAYEBIFARD, “Spark Plasma Sintering of ZrB2-SiC-ZrC Nanocomposite Synthesized by MASPS,” ADVANCED PROCESSES IN MATERIALS, vol. 14, no. 2 , pp. 1–11, 2020, [Online]. Available: https://sid.ir/paper/407844/en

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