Ultrasound-assisted emulsification solidified floating organic drop microextraction-GFAAS for determination of ultratrace aluminum: Response surface methodology and Box-Behnken Design

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Kiamarspour Sara; Abbasitabar Fatemeh

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Journal: JOURNAL OF APPLIED CHEMISTRY Year:2020 | Volume:14 | Issue:53 Page(s): 97-108

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Title

Ultrasound-assisted emulsification solidified floating organic drop microextraction-GFAAS for determination of ultratrace aluminum: Response surface methodology and Box-Behnken Design

Author(s)

Kiamarspour Sara | Abbasitabar Fatemeh | Issue Writer Certificate

Keywords

Ultrasound-assisted emulsificationQ1

MicroextractionQ1

Response surface methodologyQ1

Abstract

A simple, inexpensive and easy-to-use method of Ultrasound-assisted emulsification of solidified floating organic drops Microextraction (UAE-SFODME) coupled to GFAAS was developed for the extraction and preconcentration of aluminum. The factors affect the UAE-SFODME of aluminum, using alizarin red S (ARS) as complexing agent, were determined using one-factor-at-a time and further optimization was carried out by Box-Behnken design and Response surface methodology (RSM). Under the optimized conditions: extraction solvent 180 μ L, pH 4. 07, volume of dispersive solvent 60. 0 μ L, ARS 2. 0 mg, and sample volume of 25 mL, an enrichment factor of 80, a detection limit of 0. 16 μ g L− 1 and a relative standard deviation of 3. 5-5. 0 % were obtained. The method was effectively applied for analyzing different water samples and milk powder.

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APA: Copy

Kiamarspour, Sara, & Abbasitabar, Fatemeh. (2020). Ultrasound-assisted emulsification solidified floating organic drop microextraction-GFAAS for determination of ultratrace aluminum: Response surface methodology and Box-Behnken Design. JOURNAL OF APPLIED CHEMISTRY, 14(53 ), 97-108. SID. https://sid.ir/paper/408156/en

Vancouver: Copy

Kiamarspour Sara, Abbasitabar Fatemeh. Ultrasound-assisted emulsification solidified floating organic drop microextraction-GFAAS for determination of ultratrace aluminum: Response surface methodology and Box-Behnken Design. JOURNAL OF APPLIED CHEMISTRY[Internet]. 2020;14(53 ):97-108. Available from: https://sid.ir/paper/408156/en

IEEE: Copy

Sara Kiamarspour, and Fatemeh Abbasitabar, “Ultrasound-assisted emulsification solidified floating organic drop microextraction-GFAAS for determination of ultratrace aluminum: Response surface methodology and Box-Behnken Design,” JOURNAL OF APPLIED CHEMISTRY, vol. 14, no. 53 , pp. 97–108, 2020, [Online]. Available: https://sid.ir/paper/408156/en

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