Preconcentration and measurement of fenitrothion in water and vegetable samples using ultrasound-assisted emulsification microextraction based on applying low-density organic solvent

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KHALILIAN FAEZEH; REZAEE MOHAMMAD

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Journal: Journal of Applied Research in Chemistry Year:2021 | Volume:15 | Issue:1 Page(s): 59-68

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Information Journal Paper

Title

Preconcentration and measurement of fenitrothion in water and vegetable samples using ultrasound-assisted emulsification microextraction based on applying low-density organic solvent

Author(s)

KHALILIAN FAEZEH | REZAEE MOHAMMAD | Issue Writer Certificate

Keywords

FenitrothionQ1

Ultrasound-assisted emulsification microextractionQ1

Gas chromatography instrument Q1

Abstract

Insecticides can remain in the food products after using, and spread in the environment, surface soil and underground water. The existence of insecticides remainder in the food products is one of the most important concerns for consumers. They have undesirable effects to human health after a long time. In this research, simple and efficient Ultrasound-assisted emulsification microextraction (USAEME) method was successfully developed based on applying low density organic solvents for the extraction and determination of Fenitrothion insecticide in vegetable and water samples. Several factors influencing the extraction such as type and volume of extraction solvent, temperature, ionic strength, and centrifugation time were investigated and optimized. Under the optimum conditions, the calibration range was from 2. 0 to 100 µ g L-1 in water sample and from 0. 02 to 20 mg kg-1 in plant. The applicability of the proposed method was successfully evaluated by the extraction and determination of Fenitrothion from some natural vegetable and water samples.

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APA: Copy

KHALILIAN, FAEZEH, & REZAEE, MOHAMMAD. (2021). Preconcentration and measurement of fenitrothion in water and vegetable samples using ultrasound-assisted emulsification microextraction based on applying low-density organic solvent. JOURNAL OF APPLIED RESEARCHES IN CHEMISTRY (JARC), 15(1 ), 59-68. SID. https://sid.ir/paper/411174/en

Vancouver: Copy

KHALILIAN FAEZEH, REZAEE MOHAMMAD. Preconcentration and measurement of fenitrothion in water and vegetable samples using ultrasound-assisted emulsification microextraction based on applying low-density organic solvent. JOURNAL OF APPLIED RESEARCHES IN CHEMISTRY (JARC)[Internet]. 2021;15(1 ):59-68. Available from: https://sid.ir/paper/411174/en

IEEE: Copy

FAEZEH KHALILIAN, and MOHAMMAD REZAEE, “Preconcentration and measurement of fenitrothion in water and vegetable samples using ultrasound-assisted emulsification microextraction based on applying low-density organic solvent,” JOURNAL OF APPLIED RESEARCHES IN CHEMISTRY (JARC), vol. 15, no. 1 , pp. 59–68, 2021, [Online]. Available: https://sid.ir/paper/411174/en

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