SEPARATION OF BIOJENIC AMINES USING DANSYL CLORIDE DERIVATIZATION AND MIXED MICELLAR LIQUID CHROMATOGRAPHY

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HAJ MOHAMMADI M.R.; JAFARI S.

مرکز اطلاعات علمی Scientific Information Database (SID) - Trusted Source for Research and Academic Resources

Journal Paper

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Journal: Iranian Journal of Chemistry and Chemical Engineering Year:2006 | Volume:25 | Issue:1 Page(s): 19-23

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Title

SEPARATION OF BIOJENIC AMINES USING DANSYL CLORIDE DERIVATIZATION AND MIXED MICELLAR LIQUID CHROMATOGRAPHY

Author(s)

HAJ MOHAMMADI M.R. | JAFARI S. | Issue Writer Certificate

Keywords

BIOGENIC AMINES

HPLC

MICELLAR LIQUID CHROMATOGRAPHY

MIXED MICELLES

Abstract

Separation of some BIOGENIC AMINES via RP-HPLC using mixed micellar mobile phase was investigated. The compounds were derivatized before hand by dansyl chloride as a chromophoric reagent. Appropriate conditions for separation, were determined by studying factors such as temperature, type and percentage of organic modifier, concentration of surfactants (SDS and Brij-35) and the pH of the mobile phase. The number of theoretical plates (N), asymmetry factor (B/A) and selectivity factor (α) considered as criteria for finding the appropriate conditions for separation. Appropriate condition, were: 40˚C, 40 mM SDS, 0.5 mM Brij-35 and 10% 1-propanol at pH=5.

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APA: Copy

HAJ MOHAMMADI, M.R., & JAFARI, S.. (2006). SEPARATION OF BIOJENIC AMINES USING DANSYL CLORIDE DERIVATIZATION AND MIXED MICELLAR LIQUID CHROMATOGRAPHY . IRANIAN JOURNAL OF CHEMISTRY AND CHEMICAL ENGINEERING (IJCCE), 25(1), 19-23. SID. https://sid.ir/paper/528331/en

Vancouver: Copy

HAJ MOHAMMADI M.R., JAFARI S.. SEPARATION OF BIOJENIC AMINES USING DANSYL CLORIDE DERIVATIZATION AND MIXED MICELLAR LIQUID CHROMATOGRAPHY . IRANIAN JOURNAL OF CHEMISTRY AND CHEMICAL ENGINEERING (IJCCE)[Internet]. 2006;25(1):19-23. Available from: https://sid.ir/paper/528331/en

IEEE: Copy

M.R. HAJ MOHAMMADI, and S. JAFARI, “SEPARATION OF BIOJENIC AMINES USING DANSYL CLORIDE DERIVATIZATION AND MIXED MICELLAR LIQUID CHROMATOGRAPHY ,” IRANIAN JOURNAL OF CHEMISTRY AND CHEMICAL ENGINEERING (IJCCE), vol. 25, no. 1, pp. 19–23, 2006, [Online]. Available: https://sid.ir/paper/528331/en

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