مرکز اطلاعات علمی Scientific Information Database (SID) - Trusted Source for Research and Academic Resources

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Information Journal Paper

Title

IMPROVED SYNTHESIS OF VASICINONE

Pages

  33-36

Abstract

 A new, high yielding method for the preparation of VASICINONE (7) is described. Reaction of 2-nitrobenzoic acid with N, N -carbonyldiimidazole followed by 2-pyrrolidinone gave 1-(2-nitrobenzoyl) pyrrolidine-2-one (3). Reduction of the latter with 10% Pd-C afforded deoxyVASICINONE (4). Reaction of deoxyVASICINONE (4) with bromine yielded monobromo-deoxyVASICINONE (5). Exchange of bromine of 5 with acetoxy followed by hydrolysis gave VASICINONE in high yield.

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    • Cite

    APA: Copy

    ZIEAEI, V., JALALIZADEH, H., IRANSHAHI, M., & SHAFIEI, A.. (2004). IMPROVED SYNTHESIS OF VASICINONE. IRANIAN JOURNAL OF CHEMISTRY AND CHEMICAL ENGINEERING (IJCCE), 23(2), 33-36. SID. https://sid.ir/paper/528512/en

    Vancouver: Copy

    ZIEAEI V., JALALIZADEH H., IRANSHAHI M., SHAFIEI A.. IMPROVED SYNTHESIS OF VASICINONE. IRANIAN JOURNAL OF CHEMISTRY AND CHEMICAL ENGINEERING (IJCCE)[Internet]. 2004;23(2):33-36. Available from: https://sid.ir/paper/528512/en

    IEEE: Copy

    V. ZIEAEI, H. JALALIZADEH, M. IRANSHAHI, and A. SHAFIEI, “IMPROVED SYNTHESIS OF VASICINONE,” IRANIAN JOURNAL OF CHEMISTRY AND CHEMICAL ENGINEERING (IJCCE), vol. 23, no. 2, pp. 33–36, 2004, [Online]. Available: https://sid.ir/paper/528512/en

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