مرکز اطلاعات علمی Scientific Information Database (SID) - Trusted Source for Research and Academic Resources

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Cites:

1

Information Journal Paper

Title

ONE-POT SYNTHESIS AND CHARACTERIZATION OF HIGHLY FUNCTIONALIZED THIAZOLES

Pages

  31-37

Abstract

 A facile and efficient one-pot three-step process for the synthesis of 5-acetyl-2-imino-4-methylthiazoles via the CYCLOCONDENSATION of 3-thiocyanatoacetylacetone with various HYDRAZINE or HYDRAZIDE derivatives in EtOH has been developed.3-Thiocyanatoacetylacetone itself has been synthesized as the intermediate from substitution reaction of thiocyanate with 3-chloroacetylacetone. Better results were obtained by three-step procedures vs one-step reaction. The proposed method does not required techniques such as extraction and chromatography. Surprisingly, 3, 5-dimethyl-4-thiocyanato-1H-pyrazoles were not produced in this reaction, it was proved based on the existence of the acetyl group in the products. The molecular structures of newly synthesized compounds were elucidated on the basis of elemental analysis and spectral data.

Cites

References

Cite

APA: Copy

Beyzaei, Hamid, BEYGI, ADEL, & Aryan, Reza. (2016). ONE-POT SYNTHESIS AND CHARACTERIZATION OF HIGHLY FUNCTIONALIZED THIAZOLES. IRANIAN JOURNAL OF CHEMISTRY AND CHEMICAL ENGINEERING (IJCCE), 35(4), 31-37. SID. https://sid.ir/paper/695683/en

Vancouver: Copy

Beyzaei Hamid, BEYGI ADEL, Aryan Reza. ONE-POT SYNTHESIS AND CHARACTERIZATION OF HIGHLY FUNCTIONALIZED THIAZOLES. IRANIAN JOURNAL OF CHEMISTRY AND CHEMICAL ENGINEERING (IJCCE)[Internet]. 2016;35(4):31-37. Available from: https://sid.ir/paper/695683/en

IEEE: Copy

Hamid Beyzaei, ADEL BEYGI, and Reza Aryan, “ONE-POT SYNTHESIS AND CHARACTERIZATION OF HIGHLY FUNCTIONALIZED THIAZOLES,” IRANIAN JOURNAL OF CHEMISTRY AND CHEMICAL ENGINEERING (IJCCE), vol. 35, no. 4, pp. 31–37, 2016, [Online]. Available: https://sid.ir/paper/695683/en

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