SYNTHESIS AND CHARACTERIZATION OF NANO PARTICLES ZINC OXIDE USING HYDROTHERMAL DECOMPOSITION METHOD

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KAVOSH M.; MOALLEMIAN H. ALLAH; KOOTI M.

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Journal: JOURNAL OF SCIENCES (ISLAMIC AZAD UNIVERSITY) Year:2011 | Volume:21 | Issue:80 (CHEMISTRY ISSUE) Page(s): 25-34

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Title

SYNTHESIS AND CHARACTERIZATION OF NANO PARTICLES ZINC OXIDE USING HYDROTHERMAL DECOMPOSITION METHOD

Author(s)

KAVOSH M. | MOALLEMIAN H. ALLAH | KOOTI M. | Issue Writer Certificate

Keywords

NANOQ2

ZINC OXIDEQ2

STARCHQ2

HYDROTHERMAL DECOMPOSITIONQ2

Abstract

Introduction: ZINC OXIDE with hexagonal structure is a semiconductor which in a NANO scale has properties like as photoluminescence and laser, laser none linear and piezoelectric devices, sensitive surface to absorbers, high none linear resistance and good mechanical stability resistance.Aim: Synthesis of ZINC OXIDE NANO particles by using HYDROTHERMAL DECOMPOSITION method and evaluating effect of calcinations temperature on particle size.Material and Method: NANO particles were determined by X-ray imaging, transition electronic microscope (TEM) and scanning electronic microscope (SEM) images, absorption of UV-vis, photoluminescence (PL) and infrared (FT_IR) spectroscopy and from effective mass model and sherrer equations for the approximation of particle size were used.Results: The X-ray diffraction patterns of NANO ZINC OXIDE were compared with that of X-ray diffraction patterns ZINC OXIDE reference (JCPDS No.36-1451). Comparison of these patterns indicated that sample has crystal hexagonal structure. Images of SEM and TEM synthesized samples were admitted by forming spherical NANO particles. Also in PL analysis level of reflecting light of NANO particle were evaluated and were obtained amount of absorption and band gap energy of NANO particles synthesized by using spectroscopy UV-vis.Conclusion: Using from the polysaccharide template led to synthesize of NANOmeter-scale particle size. The results show with increasing temperature of calcinations, decreased particle size and when increasing particle size, the band gap energy decreased.

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APA: Copy

KAVOSH, M., MOALLEMIAN, H. ALLAH, & KOOTI, M.. (2011). SYNTHESIS AND CHARACTERIZATION OF NANO PARTICLES ZINC OXIDE USING HYDROTHERMAL DECOMPOSITION METHOD. JOURNAL OF SCIENCES (ISLAMIC AZAD UNIVERSITY), 21(80 (CHEMISTRY ISSUE)), 25-34. SID. https://sid.ir/paper/70571/en

Vancouver: Copy

KAVOSH M., MOALLEMIAN H. ALLAH, KOOTI M.. SYNTHESIS AND CHARACTERIZATION OF NANO PARTICLES ZINC OXIDE USING HYDROTHERMAL DECOMPOSITION METHOD. JOURNAL OF SCIENCES (ISLAMIC AZAD UNIVERSITY)[Internet]. 2011;21(80 (CHEMISTRY ISSUE)):25-34. Available from: https://sid.ir/paper/70571/en

IEEE: Copy

M. KAVOSH, H. ALLAH MOALLEMIAN, and M. KOOTI, “SYNTHESIS AND CHARACTERIZATION OF NANO PARTICLES ZINC OXIDE USING HYDROTHERMAL DECOMPOSITION METHOD,” JOURNAL OF SCIENCES (ISLAMIC AZAD UNIVERSITY), vol. 21, no. 80 (CHEMISTRY ISSUE), pp. 25–34, 2011, [Online]. Available: https://sid.ir/paper/70571/en

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