STUDY ON THE THERMAL DECOMPOSITION KINETICS AND CALCULATION OF ACTIVATION ENERGY OF DEGRADATION OF POLY (O-TOLUIDINE) USING THERMOGRAVIMETRIC ANALYSIS

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GUL HAJERA; SHAH ANWAR UL HAQ ALI; GUL SALMA; ARJOMANDI JALAL; BILAL SLAMA

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Journal: Iranian Journal of Chemistry and Chemical Engineering Year:2018 | Volume:37 | Issue:1 Page(s): 193-204

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Title

STUDY ON THE THERMAL DECOMPOSITION KINETICS AND CALCULATION OF ACTIVATION ENERGY OF DEGRADATION OF POLY (O-TOLUIDINE) USING THERMOGRAVIMETRIC ANALYSIS

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Keywords

POT

TGA

XRD

SEM

Abstract

Thermo Gravimetric Analysis (TGA) analysis was employed to investigate activation energy (Ea) for the process of degrading of poly (o-toluidine) (POT) applying Horwitz & Metzger, Coats & Redfern and Chan et al., methods. POT was synthesized by chemical oxidative polymerization method using Ammonium per Sulphate (APS) as an oxidant while Dodecylbenzene Sulphonic Acid (DBSA) and sulfuric acid as co-dopants. Different samples, synthesized by variations in the reactions parameters, were evaluated in order to choose the one with the highest activation energy of degradation. Additional characterization of the polymer was carried out through differenttechniques such as Scanning Electron Microscopy (SEM), UltraViolet Visible spectroscopy (UV-Vis)and X-Ray Diffraction (XRD) analysis.

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References

INFLUENCE OF POLYANILINE SYNTHESIS CONDITIONS ON ITS CAPABILITY FOR REMOVAL AND RECOVERY OF CHROMIUM FROM AQUEOUS SOLUTION

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APA: Copy

GUL, HAJERA, SHAH, ANWAR UL HAQ ALI, GUL, SALMA, ARJOMANDI, JALAL, & BILAL, SLAMA. (2018). STUDY ON THE THERMAL DECOMPOSITION KINETICS AND CALCULATION OF ACTIVATION ENERGY OF DEGRADATION OF POLY (O-TOLUIDINE) USING THERMOGRAVIMETRIC ANALYSIS. IRANIAN JOURNAL OF CHEMISTRY AND CHEMICAL ENGINEERING (IJCCE), 37(1), 193-204. SID. https://sid.ir/paper/714418/en

Vancouver: Copy

GUL HAJERA, SHAH ANWAR UL HAQ ALI, GUL SALMA, ARJOMANDI JALAL, BILAL SLAMA. STUDY ON THE THERMAL DECOMPOSITION KINETICS AND CALCULATION OF ACTIVATION ENERGY OF DEGRADATION OF POLY (O-TOLUIDINE) USING THERMOGRAVIMETRIC ANALYSIS. IRANIAN JOURNAL OF CHEMISTRY AND CHEMICAL ENGINEERING (IJCCE)[Internet]. 2018;37(1):193-204. Available from: https://sid.ir/paper/714418/en

IEEE: Copy

HAJERA GUL, ANWAR UL HAQ ALI SHAH, SALMA GUL, JALAL ARJOMANDI, and SLAMA BILAL, “STUDY ON THE THERMAL DECOMPOSITION KINETICS AND CALCULATION OF ACTIVATION ENERGY OF DEGRADATION OF POLY (O-TOLUIDINE) USING THERMOGRAVIMETRIC ANALYSIS,” IRANIAN JOURNAL OF CHEMISTRY AND CHEMICAL ENGINEERING (IJCCE), vol. 37, no. 1, pp. 193–204, 2018, [Online]. Available: https://sid.ir/paper/714418/en

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