ONE-POT REDUCTION OF AROMATIC CARBOXYLIC ACID TO ALCOHOL BY SIO2@FESO4 NANO COMPOSITE AT SOLVENT-FREE CONDITION

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BAGHERI MARZIYEH; KARIMKOSHTEH MOSTAFA

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Journal Paper

Paper Information

Journal: Iranian Journal of Chemistry and Chemical Engineering Year:2017 | Volume:36 | Issue:3 Page(s): 37-43

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Title

ONE-POT REDUCTION OF AROMATIC CARBOXYLIC ACID TO ALCOHOL BY SIO2@FESO4 NANO COMPOSITE AT SOLVENT-FREE CONDITION

Author(s)

BAGHERI MARZIYEH | KARIMKOSHTEH MOSTAFA | Issue Writer Certificate

Keywords

SIO2@FESO4

CARBOXYLIC ACID

ALCOHOL

NABH4

SOLVENT-FREE

Abstract

Application of SiO2@FeSO4 nano composite as a new nano catalyst in reduction area was investigated. CARBOXYLIC ACID simple and convenient reduction to ALCOHOL by 0.75 mol of the nano composite, 3 mol sodium borohydride (NaBH4) as reduction reagent under solvent free condition at 30-65 min. The reaction happens in two stages - first to form an aldehyde and then a primary ALCOHOL. Because sodium aluminum hydride reacts rapidly with aldehydes, it is impossible to stop at the halfway stage. The method does not require an anhydrous solvent, does not involve a hazardous reagent, has somewhat different selectivity than techniques in general use, and may sometimes be the method of choice.

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