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Information Journal Paper

Title

VORTEX-ASSISTED INVERTED DISPERSIVE LIQUID-LIQUID MICROEXTRACTION OF NAPROXEN FROM HUMAN PLASMA AND ITS DETERMINATION BY HIGH PERFORMANCE LIQUID CHROMATOGRAPHY

Pages

  107-114

Abstract

 Extraction and determination of NAPROXEN from human PLASMA were performed using Vortex - Assisted Inverted Dispersive Liquid–Liquid MicroExtraction (VA−IDLLME) and High Performance Liquid Chromatography (HPLC). The parameters affecting extraction recovery such as type and volume of extraction and disperser solvents, pH of sample solution, stirring rate, extraction time and salt addition were optimized. Optimal extraction conditions were: 100 mL dodecane as extraction solvent, 350 mL methanol as disperser solvent, pH of sample=5, stirring rate: 500 rpm, with no effect of extraction time and no addition of NaCl to the sample solution. Under the optimal conditions a linear range of 1.0–1000.0 ng/mL (R2=0.9993) was obtained. Limit of detection, the extraction recovery and preconcentration factor were 0.32 ng/mL, 87% and 108 respectively.

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    • Cite

    APA: Copy

    HAJMOHAMMADI, MOHAMMAD REZA, & HEMMATI, MASOUMEH. (2017). VORTEX-ASSISTED INVERTED DISPERSIVE LIQUID-LIQUID MICROEXTRACTION OF NAPROXEN FROM HUMAN PLASMA AND ITS DETERMINATION BY HIGH PERFORMANCE LIQUID CHROMATOGRAPHY. IRANIAN JOURNAL OF CHEMISTRY AND CHEMICAL ENGINEERING (IJCCE), 36(3), 107-114. SID. https://sid.ir/paper/720431/en

    Vancouver: Copy

    HAJMOHAMMADI MOHAMMAD REZA, HEMMATI MASOUMEH. VORTEX-ASSISTED INVERTED DISPERSIVE LIQUID-LIQUID MICROEXTRACTION OF NAPROXEN FROM HUMAN PLASMA AND ITS DETERMINATION BY HIGH PERFORMANCE LIQUID CHROMATOGRAPHY. IRANIAN JOURNAL OF CHEMISTRY AND CHEMICAL ENGINEERING (IJCCE)[Internet]. 2017;36(3):107-114. Available from: https://sid.ir/paper/720431/en

    IEEE: Copy

    MOHAMMAD REZA HAJMOHAMMADI, and MASOUMEH HEMMATI, “VORTEX-ASSISTED INVERTED DISPERSIVE LIQUID-LIQUID MICROEXTRACTION OF NAPROXEN FROM HUMAN PLASMA AND ITS DETERMINATION BY HIGH PERFORMANCE LIQUID CHROMATOGRAPHY,” IRANIAN JOURNAL OF CHEMISTRY AND CHEMICAL ENGINEERING (IJCCE), vol. 36, no. 3, pp. 107–114, 2017, [Online]. Available: https://sid.ir/paper/720431/en

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