A PRECURSOR TO PRODUCE PURE PHASE NANO-SIZED LEAD (II) OXIDE OF LEAD (II) COMPLEX

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ALAIE VAHID; SHAHVERDIZADEH GHOLAM HOSSEIN

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Seminar Paper

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Seminar: IRANIAN INORGANIC CHEMISTRY CONFERENCE
Year:2014 | Issue:16

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Title

A PRECURSOR TO PRODUCE PURE PHASE NANO-SIZED LEAD (II) OXIDE OF LEAD (II) COMPLEX

Author(s)

ALAIE VAHID | SHAHVERDIZADEH GHOLAM HOSSEIN | Issue Writer Certificate

Keywords

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Abstract

2-OXIDE-3-BENZALDEHYDE ISONICOTINYLHYDRAZONATO LIGANDS RELATED TO THAT IN THE TITLE COMPLEX, ARE ATTRACTING INTEREST IN THE CONTEXT OF CRYSTAL ENGINEERING ENDEAVOURS [1]. THUS FAR, THE ONLY LEAD (II) COMPLEX REPORTED WITH THIS CLASS OF LIGAND IS A BINUCLEAR COMPLEX WHERE THE PYRIDINE-N ATOM DOES NOT PARTICIPATE IN., COORDINATION [2,3]. THE PB ATOM IN THE POLYMERIC TITLE COMPOUND, {[PB(C13H9- N3O2)].CH3OH}N, IS FIVE-COORDINATED. THE COORDINATION GEOMETRY IS BASED ON A TRIGONAL BIPYRAMID WITH THE O ATOMS IN AXIAL POSITIONS. [(C13H9N3O2).CH3OH] LIGANDS RELATED TO THAT IN THE TITLE THIS COMPLEX ARE ATTRACTING INTEREST IN THE CONTEXT OF CRYSTAL ENGINEERING ENDEAVOURS [2].THE THERMAL STABILITY OF COMPOUND BOTH ITS BULK AND NANO-SIZE HAS BEEN STUDIED BY THERMAL GRAVIMETRIC (TG) AND DIFFERENTIAL THERMAL ANALYSES (DTA) AND COMPARED EACH OTHER. CALCINATION WITH AND WITHOUT SURFACTANT OF THE NANO-SIZED COMPOUND AT 400 °C AND 250 °C UNDER AIR ATMOSPHERE YIELDS LEAD (II) OXIDE NANOPARTICLES. NANO OXIDE LEAD (II) WAS CHARACTERIZED AND ANALYSIED BY SCANNING ELECTRON MICROSCOPY, X-RAY POWDER DIFFRACTION, IR SPECTROSCOPY.

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APA: Copy

ALAIE, VAHID, & SHAHVERDIZADEH, GHOLAM HOSSEIN. (2014). A PRECURSOR TO PRODUCE PURE PHASE NANO-SIZED LEAD (II) OXIDE OF LEAD (II) COMPLEX. IRANIAN INORGANIC CHEMISTRY CONFERENCE. SID. https://sid.ir/paper/910879/en

Vancouver: Copy

ALAIE VAHID, SHAHVERDIZADEH GHOLAM HOSSEIN. A PRECURSOR TO PRODUCE PURE PHASE NANO-SIZED LEAD (II) OXIDE OF LEAD (II) COMPLEX. 2014. Available from: https://sid.ir/paper/910879/en

IEEE: Copy

VAHID ALAIE, and GHOLAM HOSSEIN SHAHVERDIZADEH, “A PRECURSOR TO PRODUCE PURE PHASE NANO-SIZED LEAD (II) OXIDE OF LEAD (II) COMPLEX,” presented at the IRANIAN INORGANIC CHEMISTRY CONFERENCE. 2014, [Online]. Available: https://sid.ir/paper/910879/en

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