BIS {(3-ACETATOPROPYL) TRIPHENYLPHOSPHONIUM}TETRABROMOPALLADATE(II): SYNTHESIS, CHARACTERIZATION AND CRYSTAL STRUCTURE

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Naghipour Ali; MANSOURI GHOBAD; Haydarizadi Fatemeh; heshmatollah babaei; zahra haji ghasemi; rostami nasab farhad

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Seminar Paper

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Seminar: SYMPOSIUM OF CRYSTALLOGRAPHY AND MINERALOGY OF IRAN
Year:2016 | Issue:23

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Title

BIS {(3-ACETATOPROPYL) TRIPHENYLPHOSPHONIUM}TETRABROMOPALLADATE(II): SYNTHESIS, CHARACTERIZATION AND CRYSTAL STRUCTURE

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Abstract

FROM THE SUBSTITUTION REACTION OF TRIPHENYLPHOSPHINE AND 2-BROMO-4-HYDROXYBUTYRIC ACID G-LACTONE WITH MOLAR RATIO 1: 1 IN BENZENE SOLVENT AT ROOM TEMPERATURE, THE PHOSPHONIUM SALT CH3CO2CH2CH2CH2PPH3 +BR- HAS BEEN SYNTHESIZED. THE PREPARED PHOSPHONIUM SALT TREATED WITH PALLADIUM ACETATE (II) IN DICHLOROMETHANE AS A SOLVENT AT ROOM TEMPERATURE TO GIVE [CH3CO2CH2CH2CH2PPH3]2[PDBR4]. CHARACTERIZATION OF THE OBTAINED COMPOUND WAS PERFORMED BY ELEMENTAL ANALYSIS (CHN), IR, 1H-, 31P- AND 13C NMR TECHNIQUES AND X-RAY CRYSTALLOGRAPHY. IT IS CLEAR FROM CRYSTALLOGRAPHIC DATA THAT THIS PHOSPHONIUM COMPOUND CRYSTALLIZED IN MONOCLINIC CRYSTAL SYSTEM AND HAS SPACE GROUP P 21/C.

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APA: Copy

Naghipour, Ali, MANSOURI, GHOBAD, Haydarizadi, Fatemeh, heshmatollah, babaei, zahra, haji ghasemi, & rostami nasab, farhad. (2016). BIS {(3-ACETATOPROPYL) TRIPHENYLPHOSPHONIUM}TETRABROMOPALLADATE(II): SYNTHESIS, CHARACTERIZATION AND CRYSTAL STRUCTURE. SYMPOSIUM OF CRYSTALLOGRAPHY AND MINERALOGY OF IRAN. SID. https://sid.ir/paper/926439/en

Vancouver: Copy

Naghipour Ali, MANSOURI GHOBAD, Haydarizadi Fatemeh, heshmatollah babaei, zahra haji ghasemi, rostami nasab farhad. BIS {(3-ACETATOPROPYL) TRIPHENYLPHOSPHONIUM}TETRABROMOPALLADATE(II): SYNTHESIS, CHARACTERIZATION AND CRYSTAL STRUCTURE. 2016. Available from: https://sid.ir/paper/926439/en

IEEE: Copy

Ali Naghipour, GHOBAD MANSOURI, Fatemeh Haydarizadi, babaei heshmatollah, haji ghasemi zahra, and farhad rostami nasab, “BIS {(3-ACETATOPROPYL) TRIPHENYLPHOSPHONIUM}TETRABROMOPALLADATE(II): SYNTHESIS, CHARACTERIZATION AND CRYSTAL STRUCTURE,” presented at the SYMPOSIUM OF CRYSTALLOGRAPHY AND MINERALOGY OF IRAN. 2016, [Online]. Available: https://sid.ir/paper/926439/en

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