Diisopropyl Ether Production via Isopropanol Catalytic Dehydration over Zirconium Phosphate Modified Natural Zeolite

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Hasanudin Hasanudin; Asri Wan Ryan; Anindia Jeniva Rindi; Suheryanto Suheryanto; Fanani Zainal; Rinaldi Nino; Muttaqii Muhammad Al

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Paper Information

Journal: IRANIAN JOURNAL OF CATALYSIS Year:2022 | Volume:12 | Issue:4 Page(s): 463-474

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Title

Diisopropyl Ether Production via Isopropanol Catalytic Dehydration over Zirconium Phosphate Modified Natural Zeolite

Author(s)

Keywords

Diisopropyl ether

Iisopropanol Isopropanol conversion

Modification

Phosphate

Zeolite

Zirconium

Abstract

In this work, Diisopropyl ether (DIPE) was produced through catalytic dehydration of isopropanol over Zirconium Phosphate-modified Phosphate modified natural Zeolite. The catalyst was prepared via the wet impregnation method. They were tested at 150 ˚, C for 3 hours under a reflux system. The effect of Zeolite-Zr(H2PO4)4 metal loading and Zeolite-Zr without Phosphate incorporation on dehydration isopropanol was also assessed. The results showed the natural Zeolite was successfully modified as confirmed by XRD, FTIR, SEM-EDX, N2 physisorption, and catalyst acidity by the gravimetric technique. The highest isopropanol conversion (66. 73%) was accomplished by 8 mEq/g Zeolite-Zr(H2PO4)4 followed by the DIPE yield and selectivity up to 35. 81% and 47. 8%, respectively. Further reusability investigation showed that Zeolite-Zr(H2PO4)4 catalyst provided adequate reusability up to the fourth reused with relatively decreased catalytic activity towards isopropanol dehydration.

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APA: Copy

Hasanudin, Hasanudin, Asri, Wan Ryan, Anindia, Jeniva Rindi, Suheryanto, Suheryanto, Fanani, Zainal, Rinaldi, Nino, & Muttaqii, Muhammad Al. (2022). Diisopropyl Ether Production via Isopropanol Catalytic Dehydration over Zirconium Phosphate Modified Natural Zeolite. IRANIAN JOURNAL OF CATALYSIS, 12(4), 463-474. SID. https://sid.ir/paper/1065625/en

Vancouver: Copy

Hasanudin Hasanudin, Asri Wan Ryan, Anindia Jeniva Rindi, Suheryanto Suheryanto, Fanani Zainal, Rinaldi Nino, Muttaqii Muhammad Al. Diisopropyl Ether Production via Isopropanol Catalytic Dehydration over Zirconium Phosphate Modified Natural Zeolite. IRANIAN JOURNAL OF CATALYSIS[Internet]. 2022;12(4):463-474. Available from: https://sid.ir/paper/1065625/en

IEEE: Copy

Hasanudin Hasanudin, Wan Ryan Asri, Jeniva Rindi Anindia, Suheryanto Suheryanto, Zainal Fanani, Nino Rinaldi, and Muhammad Al Muttaqii, “Diisopropyl Ether Production via Isopropanol Catalytic Dehydration over Zirconium Phosphate Modified Natural Zeolite,” IRANIAN JOURNAL OF CATALYSIS, vol. 12, no. 4, pp. 463–474, 2022, [Online]. Available: https://sid.ir/paper/1065625/en

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