Studying the photostabilization activity of Poly(Vinyl Chloride) films containing 4-amino-5-(((5-methyl-1H-benzo[d]imidazol-2-yl)thio)methyl)-2,4-dihydro-3H-1,2,4-triazole-3-thiol with a dibutyltin complex

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Mahmood Zinah Nazih; Alias Mahasin; Kadhom Mohammed; Bakir Shaimaa Ragab; Yusop Rahimi M.; Husain Amani A.; Yousif Emad

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ISSN: 2588-4824

Journal Paper

Paper Information

Journal: POLLUTION Year:2022 | Volume:8 | Issue:3 Page(s): 1088-1102

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Title

Studying the photostabilization activity of Poly(Vinyl Chloride) films containing 4-amino-5-(((5-methyl-1H-benzo[d]imidazol-2-yl)thio)methyl)-2,4-dihydro-3H-1,2,4-triazole-3-thiol with a dibutyltin complex

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Keywords

Keywords: photochemistryQ4

triazoleQ4

organotin complexesQ4

PVCQ4

photostabilityQ4

Abstract

A new traiazole derivative (4-amino-5-(((5-methyl-1H-benzo[d]imidazol-2-yl)thio)methyl)-2,4-dihydro-3H-1,2,4-triazole-3-thiol, (L), was employed as a chelating ligand to form a dibutyltin chloride complex and improve the poly(vinyl chloride) (PVC) properties. The doped PVC films were characterized via FT-IR, UV-Vis spectrum, elemental analyses (C, H, N, and M (metallic)), and magnetic susceptibility and conductivity measurements. These characterizations were conducted at room temperature, and it was disclosed that the chelating ligand rules as a bidentate chelate. The photostabilization examination of plain and L-doped PVC films was conducted in the presence of ambient air using the accelerating weather tester, where the doping ratio was fixed to 0.5 wt.%. The photostabilization performance of the additive was evaluated by tracking the indexes of carbonyl (ICO), polyene (IPO), and hydroxyl (IOH), and weight loss relationship with irradiation time. It was noticed that the values of ICO, Ipo, and IOH enhanced with the irradiation time, where this improvement relied on the presence of the Bu2SnL complex.

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