A vanadyl complex bearing an ONO isonicotinohydrazone ligand: XRD, spectroscopy, and catalytic sulfoxidation

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Kargar Hadi; Kia Reza; Fallah Mehrjardi Mehdi

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Journal Paper

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Journal: Inorganic Chemistry Research Year:2023 | Volume:7 | Issue:1 Page(s): 59-64

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Title

A vanadyl complex bearing an ONO isonicotinohydrazone ligand: XRD, spectroscopy, and catalytic sulfoxidation

Author(s)

Kargar Hadi | Kia Reza | Fallah Mehrjardi Mehdi | Issue Writer Certificate

Keywords

tridentate Schiff base

Vanadium

SC-XRD

Homogeneous catalysis

sulfoxidation

Abstract

A new Vanadium complex was prepared by reacting [VO(acac)2] with an ONO isonicotinohydrazone ligand. Various techniques including UV-Vis, FT-IR, CHN, and SC-XRD were utilized to characterize the synthesized complex. The data collected from the diffraction study showed that the Vanadium ion is hexa-coordinated and has a distorted octahedral geometry. The VV ion is coordinated to O,N,O donor sites of the liagnd and a methoxide O atom in the equatorial positions, while methanolic and oxo O atoms occupy the axial sites. Moreover, the catalytic activity of the Vanadium complex was studied in the sulfoxidation reaction of different sulfides using hydrogen peroxide.

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