CHEMICAL REDUCTION SYNTHESIS OF COPPER NANOPARTICLES IN AQUEOUS MEDIA IN PRESENT OF MALEIC ACID AND POLYVINYLPYRROLIDONE (PVP)

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EBRAHIMZADEH F.

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Paper Information

Journal: JOURNAL OF NEW MATERIALS Year:2017 | Volume:8 | Issue:1 (29) Page(s): 121-128

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Title

CHEMICAL REDUCTION SYNTHESIS OF COPPER NANOPARTICLES IN AQUEOUS MEDIA IN PRESENT OF MALEIC ACID AND POLYVINYLPYRROLIDONE (PVP)

Author(s)

EBRAHIMZADEH F. | Issue Writer Certificate

Keywords

COPPER NANOPARTICLESQ2

HYDRAZINE HYDRATEQ2

CIS-BUTENEDIOIC ACIDQ3

POLYVINYLPYRROLIDONE (PVP)Q2

CHEMICAL REDUCTIONQ2

AQUEOUS MEDIAQ2

Abstract

The present investigation reports, novel synthesis of COPPER NANOPARTICLES with controlled size and shape in an aqueous medium via CHEMICAL REDUCTION. These syntheses accomplished using hydrazin hydrate as a reducing agent, CIS-BUTENEDIOIC ACID or Maleic acid as the surfactant and polyvinylpyrrolidone (PVP) as a capping agent. The input of extra inert gases was not necessary and this method is very simple and green. Some reaction parameters, such as amount of reactants or surfactant, pH, reaction time or rate and amount of reduction reagent, were effective character for control in the size and shape of the nanoparticles. By the analysis of UV–Vis absorption spectrum, X-ray diffraction (XRD), X-ray photoelectron spectroscopy (XPS) and energy-dispersive X-ray spectroscopy (EDX), the resultant particles were confirmed to be pure Cu with a face-centered cubic (FCC) structure. Particle morphology was characterized using Fuel emission electron microscopy (FESEM) and transmission electron microscopy (TEM). The synthesis method reported in this work might be helpful for the large-scale production of Cu nanoparticles.

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References

One-pot synthesis of size and shape controlled copper nanostructures in aqueous media and their application for fast catalytic degradation of organic dyes

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APA: Copy

EBRAHIMZADEH, F.. (2017). CHEMICAL REDUCTION SYNTHESIS OF COPPER NANOPARTICLES IN AQUEOUS MEDIA IN PRESENT OF MALEIC ACID AND POLYVINYLPYRROLIDONE (PVP). JOURNAL OF NEW MATERIALS, 8(1 (29) ), 121-128. SID. https://sid.ir/paper/169837/en

Vancouver: Copy

EBRAHIMZADEH F.. CHEMICAL REDUCTION SYNTHESIS OF COPPER NANOPARTICLES IN AQUEOUS MEDIA IN PRESENT OF MALEIC ACID AND POLYVINYLPYRROLIDONE (PVP). JOURNAL OF NEW MATERIALS[Internet]. 2017;8(1 (29) ):121-128. Available from: https://sid.ir/paper/169837/en

IEEE: Copy

F. EBRAHIMZADEH, “CHEMICAL REDUCTION SYNTHESIS OF COPPER NANOPARTICLES IN AQUEOUS MEDIA IN PRESENT OF MALEIC ACID AND POLYVINYLPYRROLIDONE (PVP),” JOURNAL OF NEW MATERIALS, vol. 8, no. 1 (29) , pp. 121–128, 2017, [Online]. Available: https://sid.ir/paper/169837/en

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