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Information Journal Paper

Title

Synthesis and identification of NiO-nanoparticles with the aid of microwave in the presence of sodium dodecyl sulfate (SDS) as a stabilizer agent and its use for the preparation of benzopyran derivatives

Pages

  125-133

Abstract

 This work reports, microwave synthesis and characterization of NiO-nanoparticles in the presence of sodium dodecyl sulfate (SDS) as a stabilizer agent. Ni(NO2)2 and NaOH powder have been used as starting reagents. Particle size distribution and characterization of products were done by X-ray diffraction (XRD), scanning electron microscopy (SEM), transmission electron microscopy (TEM) and EDX analysis. NiO-nanocomposites functional groups were deduced by FT-IR spectroscopy. Also, the efficiency of NiO-particles as a new optical material using UV-VIS spectroscopy has been evaluated. Subsequently, synthesized nanoparticles as Nanocatalyst were used for the preparation of benzopyran derivatives via one-pot three-component of dimedone, malononitrile and various types of aromatic aldehydes in methanol as solvent. The results confirmed that this nanoparticle are good catalyst for benzo-pyran synthesis after reaction condition optimization.

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  • Cite

    APA: Copy

    Sabbaghnasab, Elahe, & SHEIKHHOSSEINI, ENAYATOLLAH. (2019). Synthesis and identification of NiO-nanoparticles with the aid of microwave in the presence of sodium dodecyl sulfate (SDS) as a stabilizer agent and its use for the preparation of benzopyran derivatives. JOURNAL OF APPLIED RESEARCHES IN CHEMISTRY (JARC), 13(1 ), 125-133. SID. https://sid.ir/paper/180129/en

    Vancouver: Copy

    Sabbaghnasab Elahe, SHEIKHHOSSEINI ENAYATOLLAH. Synthesis and identification of NiO-nanoparticles with the aid of microwave in the presence of sodium dodecyl sulfate (SDS) as a stabilizer agent and its use for the preparation of benzopyran derivatives. JOURNAL OF APPLIED RESEARCHES IN CHEMISTRY (JARC)[Internet]. 2019;13(1 ):125-133. Available from: https://sid.ir/paper/180129/en

    IEEE: Copy

    Elahe Sabbaghnasab, and ENAYATOLLAH SHEIKHHOSSEINI, “Synthesis and identification of NiO-nanoparticles with the aid of microwave in the presence of sodium dodecyl sulfate (SDS) as a stabilizer agent and its use for the preparation of benzopyran derivatives,” JOURNAL OF APPLIED RESEARCHES IN CHEMISTRY (JARC), vol. 13, no. 1 , pp. 125–133, 2019, [Online]. Available: https://sid.ir/paper/180129/en

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