NEW METHOD FOR PREPARATION OF NANO ALUMINA POWDER USING ALUMINUM (III) COMPLEXES BY COMBUSTION SYNTHESIS WITHOUT FUEL

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KHOSHKHAN ZAKIYEH; SALEHI MEHDI

مرکز اطلاعات علمی Scientific Information Database (SID) - Trusted Source for Research and Academic Resources

Journal Paper

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Journal: JOURNAL OF NANOSTRUCTURES Year:2014 | Volume:4 | Issue:4 Page(s): 443-448

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Information Journal Paper

Title

NEW METHOD FOR PREPARATION OF NANO ALUMINA POWDER USING ALUMINUM (III) COMPLEXES BY COMBUSTION SYNTHESIS WITHOUT FUEL

Author(s)

KHOSHKHAN ZAKIYEH | SALEHI MEHDI | Issue Writer Certificate

Keywords

COMBUSTION METHODQ2

NANOMATERIALSQ2

ALUMINAQ2

COMPLEXQ2

FESEMQ2

Abstract

Alumina NANOMATERIALS were synthesized via a solution combustion technique using tris- (acetylacetonato) aluminum (III) COMPLEX (1) and tris- (2-formylphenolate) aluminum (III) COMPLEX (2) at 600, and 1000oC for 3h. The obtained data showed that the procedure without using fuel resulted in a better phase and morphology. To investigate the phase formation, powder X-ray diffraction technique was used. Also, FESEM micrographs were used to investigate the morphology of the obtained materials. It showed that the morphology of the obtained materials was in the form of different types of porous and particle materials. The optical properties of the obtained materials were studied by FTIR spectra. According to the data, it was found that with annealing at 600oC, the phase formation of the obtained materials showed cubic crystal structures with cell parameter a=3.14 for gamma phase. With increasing the annealing temperature to 1000oC, the obtained material was found to be in a mixture of orthorhombic and hexagonal crystal structures.

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APA: Copy

KHOSHKHAN, ZAKIYEH, & SALEHI, MEHDI. (2014). NEW METHOD FOR PREPARATION OF NANO ALUMINA POWDER USING ALUMINUM (III) COMPLEXES BY COMBUSTION SYNTHESIS WITHOUT FUEL. JOURNAL OF NANOSTRUCTURES, 4(4), 443-448. SID. https://sid.ir/paper/210909/en

Vancouver: Copy

KHOSHKHAN ZAKIYEH, SALEHI MEHDI. NEW METHOD FOR PREPARATION OF NANO ALUMINA POWDER USING ALUMINUM (III) COMPLEXES BY COMBUSTION SYNTHESIS WITHOUT FUEL. JOURNAL OF NANOSTRUCTURES[Internet]. 2014;4(4):443-448. Available from: https://sid.ir/paper/210909/en

IEEE: Copy

ZAKIYEH KHOSHKHAN, and MEHDI SALEHI, “NEW METHOD FOR PREPARATION OF NANO ALUMINA POWDER USING ALUMINUM (III) COMPLEXES BY COMBUSTION SYNTHESIS WITHOUT FUEL,” JOURNAL OF NANOSTRUCTURES, vol. 4, no. 4, pp. 443–448, 2014, [Online]. Available: https://sid.ir/paper/210909/en

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