A HIGHLY EFFICIENT SYNTHETIC METHOD FOR THE PREPARATION OF 3,4-DIMETHYLBENZALDEHYDE FROM O-XYLENE IN AQUEOUS MEDIA

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HU Y.L.; LU M.; LIU Q.F.; WEI W.; LIU X.

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ISSN: 2588-4824

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Journal: JOURNAL OF THE IRANIAN CHEMICAL SOCIETY(JICS) Year:2010 | Volume:7 | Issue:2 Page(s): 487-494

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Title

A HIGHLY EFFICIENT SYNTHETIC METHOD FOR THE PREPARATION OF 3,4-DIMETHYLBENZALDEHYDE FROM O-XYLENE IN AQUEOUS MEDIA

Author(s)

Keywords

4-DIMETHYLBENZALDEHYDE

MICELLAR CATALYSIS

PHASE TRANSFER CATALYSIS

CHLOROMETHYLATION

OXIDATION

Abstract

In this study, 3,4-DIMETHYLBENZALDEHYDE was obtained in 82.3% total yield by OXIDATION of 3,4-dimethylbenzyl chloride with NaNO3/AcOH catalyzed by PEG-600 in aqueous media. The starting material 3,4-dimethylbenzyl chloride was prepared by CHLOROMETHYLATION of o-xylene in CTAB micellar catalytic system. Compared with other synthetic methods, this method not only enhanced the yield, but also afforded an efficient work-up procedure. The structures of the products were confirmed by Elemental analysis, 1H NMR and 13C NMR or compared with authentic samples.

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APA: Copy

HU, Y.L., LU, M., LIU, Q.F., WEI, W., & LIU, X.. (2010). A HIGHLY EFFICIENT SYNTHETIC METHOD FOR THE PREPARATION OF 3,4-DIMETHYLBENZALDEHYDE FROM O-XYLENE IN AQUEOUS MEDIA. JOURNAL OF THE IRANIAN CHEMICAL SOCIETY(JICS), 7(2), 487-494. SID. https://sid.ir/paper/282379/en

Vancouver: Copy

HU Y.L., LU M., LIU Q.F., WEI W., LIU X.. A HIGHLY EFFICIENT SYNTHETIC METHOD FOR THE PREPARATION OF 3,4-DIMETHYLBENZALDEHYDE FROM O-XYLENE IN AQUEOUS MEDIA. JOURNAL OF THE IRANIAN CHEMICAL SOCIETY(JICS)[Internet]. 2010;7(2):487-494. Available from: https://sid.ir/paper/282379/en

IEEE: Copy

Y.L. HU, M. LU, Q.F. LIU, W. WEI, and X. LIU, “A HIGHLY EFFICIENT SYNTHETIC METHOD FOR THE PREPARATION OF 3,4-DIMETHYLBENZALDEHYDE FROM O-XYLENE IN AQUEOUS MEDIA,” JOURNAL OF THE IRANIAN CHEMICAL SOCIETY(JICS), vol. 7, no. 2, pp. 487–494, 2010, [Online]. Available: https://sid.ir/paper/282379/en

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