APPLICATION OF MOLECULARLY IMPRINTED POLYMER FOR SOLID PHASE EXTRACTION AND PRECONCENTRATION OF HYDROCHLOROTHIAZIDE IN PHARMACEUTICAL AND SERUM SAMPLE ANALYSIS

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REZAEI B.; MALAKPOUR S.; RAHMANIAN O.

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Journal: JOURNAL OF THE IRANIAN CHEMICAL SOCIETY(JICS) Year:2010 | Volume:7 | Issue:4 Page(s): 1004-1011

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Title

APPLICATION OF MOLECULARLY IMPRINTED POLYMER FOR SOLID PHASE EXTRACTION AND PRECONCENTRATION OF HYDROCHLOROTHIAZIDE IN PHARMACEUTICAL AND SERUM SAMPLE ANALYSIS

Author(s)

REZAEI B. | MALAKPOUR S. | RAHMANIAN O. | Issue Writer Certificate

Keywords

HYDROCHLOROTHIAZIDE

MOLECULARLY IMPRINTED POLYMER

SOLID-PHASE EXTRACTION

PRECONCENTRATION

Abstract

A new polymeric sorbent prepared by utilizing molecular imprinting technology was used for the selective extraction of HYDROCHLOROTHIAZIDE (HCT) from pharmaceutical and human serum sample. The MOLECULARLY IMPRINTED POLYMER (MIP) was prepared using HCT as the template, methacrylic acid (MAA) as the functional monomer, ethylene glycol dimethacrylate (EDMA) as the cross-linker monomer, and dimethylformamide (DMF) as a solvent. The optimized conditions of MIPs as a selective sorbent for the PRECONCENTRATION of the HCT were studied. The results showed that the drug could be quantitatively and selectively maintained in the column to be then eluted from the sorbent by using methanol-acetic acid mixture (9: 1). HCT could be determined spectrophotometrically at lmax=270 nm. This method made it possible to quantitize HCT in the range of 0.1-21.0 mg ml-1, by less than 0.55% of RSD%, with a detection limit (S/N=3) of 0.073 ng ml-1. The PRECONCENTRATION factor of 1000, recoveries of up to 96% and retention capacity of 75.0 mg g-1 were achieved using this technique.

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APA: Copy

REZAEI, B., MALAKPOUR, S., & RAHMANIAN, O.. (2010). APPLICATION OF MOLECULARLY IMPRINTED POLYMER FOR SOLID PHASE EXTRACTION AND PRECONCENTRATION OF HYDROCHLOROTHIAZIDE IN PHARMACEUTICAL AND SERUM SAMPLE ANALYSIS. JOURNAL OF THE IRANIAN CHEMICAL SOCIETY(JICS), 7(4), 1004-1011. SID. https://sid.ir/paper/282497/en

Vancouver: Copy

REZAEI B., MALAKPOUR S., RAHMANIAN O.. APPLICATION OF MOLECULARLY IMPRINTED POLYMER FOR SOLID PHASE EXTRACTION AND PRECONCENTRATION OF HYDROCHLOROTHIAZIDE IN PHARMACEUTICAL AND SERUM SAMPLE ANALYSIS. JOURNAL OF THE IRANIAN CHEMICAL SOCIETY(JICS)[Internet]. 2010;7(4):1004-1011. Available from: https://sid.ir/paper/282497/en

IEEE: Copy

B. REZAEI, S. MALAKPOUR, and O. RAHMANIAN, “APPLICATION OF MOLECULARLY IMPRINTED POLYMER FOR SOLID PHASE EXTRACTION AND PRECONCENTRATION OF HYDROCHLOROTHIAZIDE IN PHARMACEUTICAL AND SERUM SAMPLE ANALYSIS,” JOURNAL OF THE IRANIAN CHEMICAL SOCIETY(JICS), vol. 7, no. 4, pp. 1004–1011, 2010, [Online]. Available: https://sid.ir/paper/282497/en

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