SYNTHESIS OF NEW AZINES IN VARIOUS REACTION CONDITIONS AND INVESTIGATION OF THEIR CYCLOADDITION REACTION

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RANJBAR KARIMI R.; LOGHMANI KHOUZANI H.

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ISSN: 2588-4824

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Journal: JOURNAL OF THE IRANIAN CHEMICAL SOCIETY(JICS) Year:2011 | Volume:8 | Issue:1 Page(s): 223-230

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Title

SYNTHESIS OF NEW AZINES IN VARIOUS REACTION CONDITIONS AND INVESTIGATION OF THEIR CYCLOADDITION REACTION

Author(s)

RANJBAR KARIMI R. | LOGHMANI KHOUZANI H. | Issue Writer Certificate

Keywords

2-KETOALKYL QUINOLINE

AZINE

TAUTOMER

CRISS-CROSS CYCLOADDITION

DIELS-ALDER CYCLOADDITION

DIENOPHILE

Abstract

A series of new AZINEs were prepared by reaction of 2-KETOALKYL QUINOLINE derivatives with some hydrazone in solvent free reaction conditions using ultrasonic irradiation. The application of ultrasonic irradiation improved the yields and reduced the reaction times. These AZINEs, due to having -acidic hydrogen next to AZINE group and heterocycle ring, have TAUTOMERic forms the degree of each of which was determined on the basis of 13C NMR, 1H NMR, UV and IR spectrum. The results revealed that all compounds exist mostly in the enaminone form. We attempted to obtain criss-cross or probably DIELS-ALDER CYCLOADDITION products through the reaction of some of these new AZINEs with 2-chloroacrylonitrile as a DIENOPHILE. Some new diene systems developed from the said reactions.

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APA: Copy

RANJBAR KARIMI, R., & LOGHMANI KHOUZANI, H.. (2011). SYNTHESIS OF NEW AZINES IN VARIOUS REACTION CONDITIONS AND INVESTIGATION OF THEIR CYCLOADDITION REACTION. JOURNAL OF THE IRANIAN CHEMICAL SOCIETY(JICS), 8(1), 223-230. SID. https://sid.ir/paper/282530/en

Vancouver: Copy

RANJBAR KARIMI R., LOGHMANI KHOUZANI H.. SYNTHESIS OF NEW AZINES IN VARIOUS REACTION CONDITIONS AND INVESTIGATION OF THEIR CYCLOADDITION REACTION. JOURNAL OF THE IRANIAN CHEMICAL SOCIETY(JICS)[Internet]. 2011;8(1):223-230. Available from: https://sid.ir/paper/282530/en

IEEE: Copy

R. RANJBAR KARIMI, and H. LOGHMANI KHOUZANI, “SYNTHESIS OF NEW AZINES IN VARIOUS REACTION CONDITIONS AND INVESTIGATION OF THEIR CYCLOADDITION REACTION,” JOURNAL OF THE IRANIAN CHEMICAL SOCIETY(JICS), vol. 8, no. 1, pp. 223–230, 2011, [Online]. Available: https://sid.ir/paper/282530/en

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