SYNTHESIS, CRYSTAL STRUCTURE, AND PROPERTIES OF HYBRID-3D COPPER TETRAPHOSPHONATE: [CU3 ((HO3PCH2) 2N–CH2C6H4CH2–N (CH2PO3H) 2) (H2O) 4] N

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DEHGHANPOUR SAEED; REZAZADEH MARYAM; MAHMOUDI ALI; AMIR H. MAHMOUDKHANI; KHALAJ MEHDI; JAHANI KHADIJEH

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Journal: JOURNAL OF THE IRANIAN CHEMICAL SOCIETY(JICS) Year:2014 | Volume:11 | Issue:3 Page(s): 751-757

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Title

SYNTHESIS, CRYSTAL STRUCTURE, AND PROPERTIES OF HYBRID-3D COPPER TETRAPHOSPHONATE: [CU3 ((HO3PCH2) 2N–CH2C6H4CH2–N (CH2PO3H) 2) (H2O) 4] N

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Keywords

INORGANIC-ORGANIC HYBRID

MATERIALS

TETRAPHONATE

COPPER (II)

HYDROTHERMAL

Abstract

The new copper (II) tetraphosphonate, [Cu3 (HO3PCH2) 2N–CH2C6H4CH2–N (CH2PO3H) 2) (H2O) 4] n (1) was HYDROTHERMALly synthesized from the reaction of Cu (NO3) 2 and (H2O3PCH2) 2N–CH2C6H4CH2–N (CH2PO3H2) 2, (H8L). Compound 1 was structurally characterized by means of X-ray single crystal diffraction. The structure of 1 showed a 3D structure constructed from two types of Cu (II) and chelating and bridging modes of (HO3PCH2) 2N–CH2C6H4CH2–N (CH2PO3H) 2, and features a (44.610.8) topological network. The 3D compound is further stabilized by hydrogen bonds. UV–Vis diffuse reflectance and infrared spectroscopy as well as elemental analysis of compound 1 are also presented.

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APA: Copy

DEHGHANPOUR, SAEED, REZAZADEH, MARYAM, MAHMOUDI, ALI, AMIR H., MAHMOUDKHANI, KHALAJ, MEHDI, & JAHANI, KHADIJEH. (2014). SYNTHESIS, CRYSTAL STRUCTURE, AND PROPERTIES OF HYBRID-3D COPPER TETRAPHOSPHONATE: [CU₃ ((HO₃PCH₂) ₂N–CH₂C₆H₄CH₂–N (CH₂PO₃H) ₂) (H₂O) ₄] N. JOURNAL OF THE IRANIAN CHEMICAL SOCIETY(JICS), 11(3), 751-757. SID. https://sid.ir/paper/282758/en

Vancouver: Copy

DEHGHANPOUR SAEED, REZAZADEH MARYAM, MAHMOUDI ALI, AMIR H. MAHMOUDKHANI, KHALAJ MEHDI, JAHANI KHADIJEH. SYNTHESIS, CRYSTAL STRUCTURE, AND PROPERTIES OF HYBRID-3D COPPER TETRAPHOSPHONATE: [CU₃ ((HO₃PCH₂) ₂N–CH₂C₆H₄CH₂–N (CH₂PO₃H) ₂) (H₂O) ₄] N. JOURNAL OF THE IRANIAN CHEMICAL SOCIETY(JICS)[Internet]. 2014;11(3):751-757. Available from: https://sid.ir/paper/282758/en

IEEE: Copy

SAEED DEHGHANPOUR, MARYAM REZAZADEH, ALI MAHMOUDI, MAHMOUDKHANI AMIR H., MEHDI KHALAJ, and KHADIJEH JAHANI, “SYNTHESIS, CRYSTAL STRUCTURE, AND PROPERTIES OF HYBRID-3D COPPER TETRAPHOSPHONATE: [CU₃ ((HO₃PCH₂) ₂N–CH₂C₆H₄CH₂–N (CH₂PO₃H) ₂) (H₂O) ₄] N,” JOURNAL OF THE IRANIAN CHEMICAL SOCIETY(JICS), vol. 11, no. 3, pp. 751–757, 2014, [Online]. Available: https://sid.ir/paper/282758/en