A THREE-DIMENSIONAL POROUS AND MAGNETIC FRAMEWORK CONSTRUCTED FROM COPPER SALT AND 5-METHYLTETRAZOLE: [CU8 (METZ) 9] (OH) XH2 O

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LIU DONG SHENG; WANG JINGWEI; ZHANG LIMING; CHEN WEN TONG; HUANG JIAN GEN; SUI YAN

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Journal: JOURNAL OF THE IRANIAN CHEMICAL SOCIETY(JICS) Year:2014 | Volume:11 | Issue:3 Page(s): 847-852

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Title

A THREE-DIMENSIONAL POROUS AND MAGNETIC FRAMEWORK CONSTRUCTED FROM COPPER SALT AND 5-METHYLTETRAZOLE: [CU8 (METZ) 9] (OH) XH2 O

Author(s)

Keywords

CUI

II COMPLEX

5-METHYLTETRAZOLE

ADSORPTION

MAGNETIC PROPERTIES

Abstract

A new compound of [Cu8 (Metz) 9] (OH)·xH2O (x »3) (1) (Metz = 5-METHYLTETRAZOLE) has been prepared and characterized by elemental analysis, IR spectroscopy and single-crystal X-ray diffraction. The crystal is of hexagonal, space group P63/m with a = b = 13.988(1) Å, c = 16.309 (2)Å, a = b = 90o, g= 120o, V = 2 763.5 (4) Å3, Mr = 1327.13, Dc = 1.595 g cm−3, Z = 2, F(000) = 1 316, m= 3.076 mm−1, the final R = 0.0494 and wR = 0.1532 for 1,731 observed reflections (I > 2 s(I)). In this compound, the [(CuII) 2 (CuI) 6 (Metz) 9]+ cationic clusters are connected together through CuI cations and Metz ligands and result in a three-dimensional framework. Remarkable, three-dimensional intersecting channels exist in it. The variable temperature magnetic investigations indicate that 1 exhibits typical antiferromagnetic behaviors. N2 gas ADSORPTION measurements at 77 K showed that compound 1 possesses permanent porosities.

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APA: Copy

LIU, DONG SHENG, WANG, JINGWEI, ZHANG, LIMING, CHEN, WEN TONG, HUANG, JIAN GEN, & SUI, YAN. (2014). A THREE-DIMENSIONAL POROUS AND MAGNETIC FRAMEWORK CONSTRUCTED FROM COPPER SALT AND 5-METHYLTETRAZOLE: [CU₈ (METZ) ₉] (OH) XH₂ O. JOURNAL OF THE IRANIAN CHEMICAL SOCIETY(JICS), 11(3), 847-852. SID. https://sid.ir/paper/282762/en

Vancouver: Copy

LIU DONG SHENG, WANG JINGWEI, ZHANG LIMING, CHEN WEN TONG, HUANG JIAN GEN, SUI YAN. A THREE-DIMENSIONAL POROUS AND MAGNETIC FRAMEWORK CONSTRUCTED FROM COPPER SALT AND 5-METHYLTETRAZOLE: [CU₈ (METZ) ₉] (OH) XH₂ O. JOURNAL OF THE IRANIAN CHEMICAL SOCIETY(JICS)[Internet]. 2014;11(3):847-852. Available from: https://sid.ir/paper/282762/en

IEEE: Copy

DONG SHENG LIU, JINGWEI WANG, LIMING ZHANG, WEN TONG CHEN, JIAN GEN HUANG, and YAN SUI, “A THREE-DIMENSIONAL POROUS AND MAGNETIC FRAMEWORK CONSTRUCTED FROM COPPER SALT AND 5-METHYLTETRAZOLE: [CU₈ (METZ) ₉] (OH) XH₂ O,” JOURNAL OF THE IRANIAN CHEMICAL SOCIETY(JICS), vol. 11, no. 3, pp. 847–852, 2014, [Online]. Available: https://sid.ir/paper/282762/en

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