APPLICATION OF A SENSITIVE NANOCOMPOSITE-BASED ELECTROCHEMICAL SENSOR FOR VOLTAMMETRIC DETERMINATION OF DICYCLOMINE HYDROCHLORIDE IN REAL SAMPLES

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MADRAKIAN TAYYEBEH; MALEKI SOMAYEH; AFKHAMI ABBAS

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Journal: JOURNAL OF THE IRANIAN CHEMICAL SOCIETY(JICS) Year:2016 | Volume:13 | Issue:10 Page(s): 0-0

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Title

APPLICATION OF A SENSITIVE NANOCOMPOSITE-BASED ELECTROCHEMICAL SENSOR FOR VOLTAMMETRIC DETERMINATION OF DICYCLOMINE HYDROCHLORIDE IN REAL SAMPLES

Author(s)

MADRAKIAN TAYYEBEH | MALEKI SOMAYEH | AFKHAMI ABBAS | Issue Writer Certificate

Keywords

GOLD NANO PARTICLES MULTI WALLED CARBON NANOTUBES DICYCLOMINE HYDROCHLORIDE DIFFERENTIAL PULSE VOLTAMMETRY ELECTROCHEMICAL SENSOR

Abstract

In the present study a glassy carbon electrode, modified with nanocomposite of gold nanoparticles/multiwalled carbon nanotubes (GNPs/MWCNTs/GCE), was used for determination of dicyclomine hydrochloride (DcCl). The results showed that synergetic effects of GNPs and MWCNTs highly improved electrochemical response and sensitivity of the sensor. The electrochemical oxidation of DcCl was investigated by cyclic voltammetry and differential pulse voltammetry. Also, scanning electron microscopy and energy dispersive x-ray spectroscopy were used to evaluate microstructure of electrochemical sensor. The effect of various experimental parameters including pH and scan rate on the voltammetric response of DcCl were investigated. Under the optimal conditions linear response was observed in range of 1.0-1.2 × 102 mmol L-1 for DcCl. The lower detection limit was found to be 0.40 µmol L-1 for DcCl. The investigated method showed good stability, reproducibility and repeatability. The proposed sensor was successfully applied to the determination of DcCl in real samples.

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APA: Copy

MADRAKIAN, TAYYEBEH, MALEKI, SOMAYEH, & AFKHAMI, ABBAS. (2016). APPLICATION OF A SENSITIVE NANOCOMPOSITE-BASED ELECTROCHEMICAL SENSOR FOR VOLTAMMETRIC DETERMINATION OF DICYCLOMINE HYDROCHLORIDE IN REAL SAMPLES. JOURNAL OF THE IRANIAN CHEMICAL SOCIETY(JICS), 13(10), 0-0. SID. https://sid.ir/paper/283231/en

Vancouver: Copy

MADRAKIAN TAYYEBEH, MALEKI SOMAYEH, AFKHAMI ABBAS. APPLICATION OF A SENSITIVE NANOCOMPOSITE-BASED ELECTROCHEMICAL SENSOR FOR VOLTAMMETRIC DETERMINATION OF DICYCLOMINE HYDROCHLORIDE IN REAL SAMPLES. JOURNAL OF THE IRANIAN CHEMICAL SOCIETY(JICS)[Internet]. 2016;13(10):0-0. Available from: https://sid.ir/paper/283231/en

IEEE: Copy

TAYYEBEH MADRAKIAN, SOMAYEH MALEKI, and ABBAS AFKHAMI, “APPLICATION OF A SENSITIVE NANOCOMPOSITE-BASED ELECTROCHEMICAL SENSOR FOR VOLTAMMETRIC DETERMINATION OF DICYCLOMINE HYDROCHLORIDE IN REAL SAMPLES,” JOURNAL OF THE IRANIAN CHEMICAL SOCIETY(JICS), vol. 13, no. 10, pp. 0–0, 2016, [Online]. Available: https://sid.ir/paper/283231/en

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