POLYURETHANE COMPOSITE ADSORBENT USING SOLID PHASE EXTRACTION METHOD FOR PRECONCENTRATION OF METAL ION FROM AQUEOUS SOLUTION

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OLORUNDARE O.F.; MSAGATI T.A.M.; KRAUSE R.W.M.; OKONKWO J.O.; MAMBA B.B.

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Journal Paper

Paper Information

Journal: INTERNATIONAL JOURNAL OF ENVIRONMENTAL SCIENCE AND TECHNOLOGY (IJEST) Year:2015 | Volume:12 | Issue:7 Page(s): 0-0

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Title

POLYURETHANE COMPOSITE ADSORBENT USING SOLID PHASE EXTRACTION METHOD FOR PRECONCENTRATION OF METAL ION FROM AQUEOUS SOLUTION

Author(s)

OLORUNDARE O.F. | MSAGATI T.A.M. | KRAUSE R.W.M. | OKONKWO J.O. | MAMBA B.B.

Keywords

HEAVY METALS

POLYMER ADSORBENT COMPOSITE (PCAD)

PRECONCENTRATION SOLID

PHASE EXTRACTION (SPE)

INDUCTIVELY COUPLED PLASMA OPTICAL EMISSION SPECTROSCOPY (ICP-OES)

Abstract

Polyurethane composite adsorbent polymeric material was prepared and investigated for selected solid-phase extraction for metal ions, prior to its determination by inductively coupled plasma optical emission spectrometry. The surface characterisation was done using Fourier transform infrared spectroscopy. The separation and preconcentration conditions of the analytes investigated includes influence of pH, sample loading flow rate, elution flow rate, type and concentration of eluents. The optimum pH for the highest efficient recoveries for all metal ions, which ranged from 70 to 85%, is pH 7. The metal ions were quantitatively eluted with 5 mL of 2 mol/L HNO3. Common coexisting ions did not interfere with the separation. The percentage recovery of the metal ions ranged between 70 and 89%, while the results for the limit of detection and limit of quantification ranged from 0.249 to 0.256 and 0.831 to 0.855, respectively. The experimental tests showed good preconcentration results of trace levels of metal ions using synthesised polyurethane polymer adsorbent composite.

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APA: Copy

OLORUNDARE, O.F., MSAGATI, T.A.M., KRAUSE, R.W.M., OKONKWO, J.O., & MAMBA, B.B.. (2015). POLYURETHANE COMPOSITE ADSORBENT USING SOLID PHASE EXTRACTION METHOD FOR PRECONCENTRATION OF METAL ION FROM AQUEOUS SOLUTION. INTERNATIONAL JOURNAL OF ENVIRONMENTAL SCIENCE AND TECHNOLOGY (IJEST), 12(7), 0-0. SID. https://sid.ir/paper/286102/en

Vancouver: Copy

OLORUNDARE O.F., MSAGATI T.A.M., KRAUSE R.W.M., OKONKWO J.O., MAMBA B.B.. POLYURETHANE COMPOSITE ADSORBENT USING SOLID PHASE EXTRACTION METHOD FOR PRECONCENTRATION OF METAL ION FROM AQUEOUS SOLUTION. INTERNATIONAL JOURNAL OF ENVIRONMENTAL SCIENCE AND TECHNOLOGY (IJEST)[Internet]. 2015;12(7):0-0. Available from: https://sid.ir/paper/286102/en

IEEE: Copy

O.F. OLORUNDARE, T.A.M. MSAGATI, R.W.M. KRAUSE, J.O. OKONKWO, and B.B. MAMBA, “POLYURETHANE COMPOSITE ADSORBENT USING SOLID PHASE EXTRACTION METHOD FOR PRECONCENTRATION OF METAL ION FROM AQUEOUS SOLUTION,” INTERNATIONAL JOURNAL OF ENVIRONMENTAL SCIENCE AND TECHNOLOGY (IJEST), vol. 12, no. 7, pp. 0–0, 2015, [Online]. Available: https://sid.ir/paper/286102/en

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