Synthesis, Characterization, Fluorescence and Electrochemical Studies of New Ferrocene Schiff base ligand Containing Nitrogen Donor Atoms and Its Palladium(II), Nickel(II) and Copper(II) Complexes

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ABBASI PARVANEH; Shafaatian Bita

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Journal: Applied Chemistry Today Year:2020 | Volume:15 | Issue:55 Page(s): 111-123

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Title

Synthesis, Characterization, Fluorescence and Electrochemical Studies of New Ferrocene Schiff base ligand Containing Nitrogen Donor Atoms and Its Palladium(II), Nickel(II) and Copper(II) Complexes

Author(s)

ABBASI PARVANEH | Shafaatian Bita | Issue Writer Certificate

Keywords

Schiff baseQ1

FerroceneQ1

Nickel(II) complexQ1

copper(II) complexQ1

FluorescenceQ1

ElectrochemistryQ1

Abstract

A new bidentate Schiff base ligand was derived from the 2: 1 molar condensation of Ferrocenecarboxaldehyde with 3, 4-diaminobenzophenone. Palladium, nickel and copper complexes were obtained by the reaction of the bidentate Schiff base ligand with palladium(II) acetate, nickel(II) acetate tetrahydrate and copper(II) acetate monohydrate in 1: 1 molar ratio. In palladium, nickel and copper complexes the ligand was coordinated to metals via the imine N atoms. The Fluorescence properties of the Schiff base ligand and its complexes were studied in DMSO. The molar conductivity values of complexes in acetone solvent implied the presence of non-electrolyte species. Electrochemical properties of the ligand and its metal complexes were investigated in the DMSO solvent at the 100 mVs− 1 scan rate. The ligand and its metal complexes showed both reversible and irreversible processes at this scan rate. The products were characterized by FT-IR, 1H NMR, UV-Vis spectroscopies, elemental analysis, and conductometry.

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APA: Copy

ABBASI, PARVANEH, & Shafaatian, Bita. (2020). Synthesis, Characterization, Fluorescence and Electrochemical Studies of New Ferrocene Schiff base ligand Containing Nitrogen Donor Atoms and Its Palladium(II), Nickel(II) and Copper(II) Complexes. JOURNAL OF APPLIED CHEMISTRY, 15(55 ), 111-123. SID. https://sid.ir/paper/381947/en

Vancouver: Copy

ABBASI PARVANEH, Shafaatian Bita. Synthesis, Characterization, Fluorescence and Electrochemical Studies of New Ferrocene Schiff base ligand Containing Nitrogen Donor Atoms and Its Palladium(II), Nickel(II) and Copper(II) Complexes. JOURNAL OF APPLIED CHEMISTRY[Internet]. 2020;15(55 ):111-123. Available from: https://sid.ir/paper/381947/en

IEEE: Copy

PARVANEH ABBASI, and Bita Shafaatian, “Synthesis, Characterization, Fluorescence and Electrochemical Studies of New Ferrocene Schiff base ligand Containing Nitrogen Donor Atoms and Its Palladium(II), Nickel(II) and Copper(II) Complexes,” JOURNAL OF APPLIED CHEMISTRY, vol. 15, no. 55 , pp. 111–123, 2020, [Online]. Available: https://sid.ir/paper/381947/en

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