Effect of drying temperature on structural, dielectric, optical and magnetic properties of sol-gel derived BiFeO3 nanoparticles

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RANJBAR MOHAMMAD; Ghazi mohammad Ebrahim; Izadifard Morteza

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Journal: Iranian Journal of Crystallography and Mineralogy Year:2018 | Volume:26 | Issue:1 Page(s): 251-260

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Information Journal Paper

Title

Effect of drying temperature on structural, dielectric, optical and magnetic properties of sol-gel derived BiFeO3 nanoparticles

Author(s)

RANJBAR MOHAMMAD | Ghazi mohammad Ebrahim | Izadifard Morteza | Issue Writer Certificate

Keywords

4-nitrosulfonyl hydrazideQ1

Schiff baseQ1

cocrystalQ1

Crystal structureQ2

Abstract

The reaction of 2-hydroxy-3-methoxybenzaldehyde with 4-nitrosulfonylhydrazide under refluxing led to co-crystalline compound contains N'-(2-hydroxy-3-methoxy benzylidene)-4-nitro benzenesulfonylhydrazide (a sulfonamide-Schiff base compound) and 1, 2-bis (2-hydroxy-3-methoxy-benzylidenehydrazine) (I). A medium strong hydrogen bonds in 1 links the oxygen atoms of one molecule of 1, 2-bis(2-hydroxy-3-methoxy-benzylidenehydrazine) to the NH group of the N'-(2-hydroxy-3-methoxy benzylidene)-4-nitrobenzenesulfonylhydrazide and is responsible for establishing of co-crystals. Compound 1 was characterized by NMR and IR spectroscopy, elemental analysis and single crystal X-ray diffraction method. Crystallographic data for 1 was collected at 95 K. The synthesized compound has been crystallized in monoclinic system with P21/n space group and a = 6. 6771(2) Å , b = 19. 2072(6) Å , c = 17. 3980(1) Å , β = 95. 56(3)º cell parameters. The final R value is 0. 037 for 07 independent reflections.

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APA: Copy

RANJBAR, MOHAMMAD, Ghazi, mohammad Ebrahim, & Izadifard, Morteza. (2018). Effect of drying temperature on structural, dielectric, optical and magnetic properties of sol-gel derived BiFeO3 nanoparticles. IRANIAN JOURNAL OF CRYSTALLOGRAPHY AND MINERALOGY, 26(1 ), 251-260. SID. https://sid.ir/paper/396567/en

Vancouver: Copy

RANJBAR MOHAMMAD, Ghazi mohammad Ebrahim, Izadifard Morteza. Effect of drying temperature on structural, dielectric, optical and magnetic properties of sol-gel derived BiFeO3 nanoparticles. IRANIAN JOURNAL OF CRYSTALLOGRAPHY AND MINERALOGY[Internet]. 2018;26(1 ):251-260. Available from: https://sid.ir/paper/396567/en

IEEE: Copy

MOHAMMAD RANJBAR, mohammad Ebrahim Ghazi, and Morteza Izadifard, “Effect of drying temperature on structural, dielectric, optical and magnetic properties of sol-gel derived BiFeO3 nanoparticles,” IRANIAN JOURNAL OF CRYSTALLOGRAPHY AND MINERALOGY, vol. 26, no. 1 , pp. 251–260, 2018, [Online]. Available: https://sid.ir/paper/396567/en

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