Crystal Structure of N'-(2-hydroxy-3-methoxy benzylidene)-4-nitro benzenesulfonylhydrazide and 1, 2-bis(2-hydroxy-3-methoxy-benzylidenehydrazine) as a co-crystalline compound

Q: How can I download an article?

To download an article from SID, first log in to the site, search for the article title, and click on the 'Download Article' option.

Q: How can I download an ISI article?

To download an ISI article on SID, enter the keyword or article title in the search bar, view the relevant results, click on the desired article, and select the 'Download Article' option.

Q: How can I access the SID database?

To access the SID database, visit SID.ir, create an account, and log in to access scientific resources.

Q: Is downloading articles from SID free?

Some articles on SID are available for free, while others require payment. Details are specified on the article's page.

TAHRIRI MOZHGAN; Tabatabaei Masuome; YOUSEFI MOHAMMAD; Mehrani khalil; Dehghani Ashkezari Mahmoud; Dusek mikaeil

مرکز اطلاعات علمی Scientific Information Database (SID) - Trusted Source for Research and Academic Resources

Journal Paper

Paper Information

Journal: Iranian Journal of Crystallography and Mineralogy Year:2018 | Volume:26 | Issue:1 Page(s): 245-250

Download Full-Text

Persian Verion

View:

202

Download:

Cites:

Information Journal Paper

Title

Crystal Structure of N'-(2-hydroxy-3-methoxy benzylidene)-4-nitro benzenesulfonylhydrazide and 1, 2-bis(2-hydroxy-3-methoxy-benzylidenehydrazine) as a co-crystalline compound

Author(s)

Keywords

4-nitrosulfonyl hydrazideQ1

Schiff baseQ2

cocrystalQ1

Crystal structureQ2

Abstract

The reaction of 2-hydroxy-3-methoxybenzaldehyde with 4-nitrosulfonylhydrazide under refluxing led to co-crystalline compound contains N'-(2-hydroxy-3-methoxy benzylidene)-4-nitro benzenesulfonylhydrazide (a sulfonamide-Schiff base compound) and 1, 2-bis (2-hydroxy-3-methoxy-benzylidenehydrazine) (I). A medium strong hydrogen bonds in 1 links the oxygen atoms of one molecule of 1, 2-bis(2-hydroxy-3-methoxy-benzylidenehydrazine) to the NH group of the N'-(2-hydroxy-3-methoxy benzylidene)-4-nitrobenzenesulfonylhydrazide and is responsible for establishing of co-crystals. Compound 1 was characterized by NMR and IR spectroscopy, elemental analysis and single crystal X-ray diffraction method. Crystallographic data for 1 was collected at 95 K. The synthesized compound has been crystallized in monoclinic system with P21/n space group and a = 6. 6771(2) Å , b = 19. 2072(6) Å , c = 17. 3980(1) Å , β = 95. 56(3)º cell parameters. The final R value is 0. 037 for 07 independent reflections.

Cites

No record.

References

No record.

Cite

APA: Copy

TAHRIRI, MOZHGAN, Tabatabaei, Masuome, YOUSEFI, MOHAMMAD, Mehrani, khalil, Dehghani Ashkezari, Mahmoud, & Dusek, mikaeil. (2018). Crystal Structure of N'-(2-hydroxy-3-methoxy benzylidene)-4-nitro benzenesulfonylhydrazide and 1, 2-bis(2-hydroxy-3-methoxy-benzylidenehydrazine) as a co-crystalline compound. IRANIAN JOURNAL OF CRYSTALLOGRAPHY AND MINERALOGY, 26(1 ), 245-250. SID. https://sid.ir/paper/403045/en

Vancouver: Copy

TAHRIRI MOZHGAN, Tabatabaei Masuome, YOUSEFI MOHAMMAD, Mehrani khalil, Dehghani Ashkezari Mahmoud, Dusek mikaeil. Crystal Structure of N'-(2-hydroxy-3-methoxy benzylidene)-4-nitro benzenesulfonylhydrazide and 1, 2-bis(2-hydroxy-3-methoxy-benzylidenehydrazine) as a co-crystalline compound. IRANIAN JOURNAL OF CRYSTALLOGRAPHY AND MINERALOGY[Internet]. 2018;26(1 ):245-250. Available from: https://sid.ir/paper/403045/en

IEEE: Copy

MOZHGAN TAHRIRI, Masuome Tabatabaei, MOHAMMAD YOUSEFI, khalil Mehrani, Mahmoud Dehghani Ashkezari, and mikaeil Dusek, “Crystal Structure of N'-(2-hydroxy-3-methoxy benzylidene)-4-nitro benzenesulfonylhydrazide and 1, 2-bis(2-hydroxy-3-methoxy-benzylidenehydrazine) as a co-crystalline compound,” IRANIAN JOURNAL OF CRYSTALLOGRAPHY AND MINERALOGY, vol. 26, no. 1 , pp. 245–250, 2018, [Online]. Available: https://sid.ir/paper/403045/en

Related Journal Papers

No record.

Related Seminar Papers

No record.

Related Plans

No record.

Recommended Workshops