PREPARATION AND MICROSTRUCTURE CHARACTERIZATION OF NANOSTRUCTURE FORSTERITE POWDER

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AGHDAEE S.R.; SADEGHI Z.M.

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Journal: Iranian Journal of Crystallography and Mineralogy Year:2012 | Volume:20 | Issue:2 Page(s): 365-374

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Information Journal Paper

Title

PREPARATION AND MICROSTRUCTURE CHARACTERIZATION OF NANOSTRUCTURE FORSTERITE POWDER

Author(s)

AGHDAEE S.R. | SADEGHI Z.M. | Issue Writer Certificate

Keywords

MG2SIO4 (FORSTERITE)Q2

NANO POWDERQ2

RIETVELD METHODQ2

MICROSTRUCTUREQ2

ANNEALING TEMPERATUREQ2

Abstract

Nanostructure Forsterite powder was prepared by Sol-gel method and its MICROSTRUCTURE was studied at a number of ANNEALING TEMPERATUREs using Rietveld structure and MICROSTRUCTURE refinements. It was found that Sol-gel method used in this experiment does not produce pure Mg2SiO4 NANO POWDER. Instead the product is a mixture of Mg2SiO4 and MgO phases with approximate weight fractions of 75% and 25%, respectively. X-ray diffraction line broadening analysis revealed the crystallite shape is nearly spherical with the volume weighted average size of 20–50 nm in the ANNEALING TEMPERATURE range of 800–1100 oC. More investigations considering anisotropic line broadening confirmed the crystallite size and lattice strain are hkl dependent, but the anisotropy of strain is more pronounced.

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APA: Copy

AGHDAEE, S.R., & SADEGHI, Z.M.. (2012). PREPARATION AND MICROSTRUCTURE CHARACTERIZATION OF NANOSTRUCTURE FORSTERITE POWDER. IRANIAN JOURNAL OF CRYSTALLOGRAPHY AND MINERALOGY, 20(2), 365-374. SID. https://sid.ir/paper/4132/en

Vancouver: Copy

AGHDAEE S.R., SADEGHI Z.M.. PREPARATION AND MICROSTRUCTURE CHARACTERIZATION OF NANOSTRUCTURE FORSTERITE POWDER. IRANIAN JOURNAL OF CRYSTALLOGRAPHY AND MINERALOGY[Internet]. 2012;20(2):365-374. Available from: https://sid.ir/paper/4132/en

IEEE: Copy

S.R. AGHDAEE, and Z.M. SADEGHI, “PREPARATION AND MICROSTRUCTURE CHARACTERIZATION OF NANOSTRUCTURE FORSTERITE POWDER,” IRANIAN JOURNAL OF CRYSTALLOGRAPHY AND MINERALOGY, vol. 20, no. 2, pp. 365–374, 2012, [Online]. Available: https://sid.ir/paper/4132/en

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