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Information Journal Paper

Title

CONTINUOUS SYNTHESIS OF OLEYL OLEATE IN SUPERCRITICAL CARBON DIOXIDE USING SOLID P-TOLUENESULFONIC ACID AS CATALYST

Pages

  79-83

Abstract

 SUPERCRITICAL CARBON DIOXIDE (SC-CO2) was used as solvent to synthesize OLEYL OLEATE as an analog of JOJOBA OIL from oleic acid and oleyl alcohol with high conversion (100%) of the acid into ester in a short time of 100 min. Utilizing a low cost solid catalyst, P-TOLUENESULFONIC ACID monohydrate (PTSA), the ESTERIFICATION REACTION was performed, without any prior preparation step, in a flow mode, at a pressure of 147 bar and a temperature of 60 degreesC. This method seems industrially suitable for the production of OLEYL OLEATE. The solubility of a mixture of oleyl alcohol and oleic acid in SC-CO2 were also measured to calculate the alcohol to acid ratio and the esterification yield.

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    • Cite

    APA: Copy

    GHAZIASKAR, S.H., & IKUSHIMA, Y.. (2000). CONTINUOUS SYNTHESIS OF OLEYL OLEATE IN SUPERCRITICAL CARBON DIOXIDE USING SOLID P-TOLUENESULFONIC ACID AS CATALYST. IRANIAN JOURNAL OF CHEMISTRY AND CHEMICAL ENGINEERING (IJCCE), 19(2), 79-83. SID. https://sid.ir/paper/539895/en

    Vancouver: Copy

    GHAZIASKAR S.H., IKUSHIMA Y.. CONTINUOUS SYNTHESIS OF OLEYL OLEATE IN SUPERCRITICAL CARBON DIOXIDE USING SOLID P-TOLUENESULFONIC ACID AS CATALYST. IRANIAN JOURNAL OF CHEMISTRY AND CHEMICAL ENGINEERING (IJCCE)[Internet]. 2000;19(2):79-83. Available from: https://sid.ir/paper/539895/en

    IEEE: Copy

    S.H. GHAZIASKAR, and Y. IKUSHIMA, “CONTINUOUS SYNTHESIS OF OLEYL OLEATE IN SUPERCRITICAL CARBON DIOXIDE USING SOLID P-TOLUENESULFONIC ACID AS CATALYST,” IRANIAN JOURNAL OF CHEMISTRY AND CHEMICAL ENGINEERING (IJCCE), vol. 19, no. 2, pp. 79–83, 2000, [Online]. Available: https://sid.ir/paper/539895/en

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