Size Optimization of Silver Nanoparticles Synthesized by Gelcasting using the Taguchi Method

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Askari Zadeh Mahani Ali; MANTEGHIAN MEHRDAD

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Journal Paper

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Journal: JOURNAL OF NANOSTRUCTURES Year:2019 | Volume:9 | Issue:3 Page(s): 468-477

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Title

Size Optimization of Silver Nanoparticles Synthesized by Gelcasting using the Taguchi Method

Author(s)

Askari Zadeh Mahani Ali | MANTEGHIAN MEHRDAD | Issue Writer Certificate

Keywords

Gelcasting

Silver Nanoparticles

Taguchi Method

Abstract

In the present study, Silver Nanoparticles were synthesized by decomposition of AgNO3 via Gelcasting. Methacrylamide was used as a low toxic monomer for gel formation. Effect of monomer content (MAM), crosslinker to monomer ratio (MBAM/MAM), silver salt to monomer ratio (AgNO3/MAM), duration of calcination, and temperature of calcination were investigated to optimize the size of nanoparticles. Taguchi Method was applied to study the effect of Gelcasting parameters on the size of Silver Nanoparticles. Mentioned parameters were surveyed at four levels and based on the Taguchi Method 16 experiments were carried out. Silver Nanoparticles were characterized, and average particle sizes were measured by SEM analysis. By using the signal to noise ratio (S/N) analysis of the results, it is revealed that monomer content is the most effective parameter on size of particles. Also, optimal values of monomer content, cross-linker to monomer ratio, silver salt to monomer ratio, duration of calcination and temperature of calcination for the minimum particle size were found to be 4. 25 g (in 20 g water), 1: 3, 1: 15, 6 h and 650⁰ C, respectively. An evaluation test was performed with the optimal value of parameters, and suitable agreement between the prediction and experimental results was observed.

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APA: Copy

Askari Zadeh Mahani, Ali, & MANTEGHIAN, MEHRDAD. (2019). Size Optimization of Silver Nanoparticles Synthesized by Gelcasting using the Taguchi Method. JOURNAL OF NANOSTRUCTURES, 9(3), 468-477. SID. https://sid.ir/paper/734322/en

Vancouver: Copy

Askari Zadeh Mahani Ali, MANTEGHIAN MEHRDAD. Size Optimization of Silver Nanoparticles Synthesized by Gelcasting using the Taguchi Method. JOURNAL OF NANOSTRUCTURES[Internet]. 2019;9(3):468-477. Available from: https://sid.ir/paper/734322/en

IEEE: Copy

Ali Askari Zadeh Mahani, and MEHRDAD MANTEGHIAN, “Size Optimization of Silver Nanoparticles Synthesized by Gelcasting using the Taguchi Method,” JOURNAL OF NANOSTRUCTURES, vol. 9, no. 3, pp. 468–477, 2019, [Online]. Available: https://sid.ir/paper/734322/en

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