Synthesis and Crystal Structure of [Pb(gly)2]n; New lead(II) Coordination Polymer with Glycine Ligand

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shokhchashm Zarnoosh; Hakimifar Azar; HASHEMI LIDA; MORSALI ALI; DUSEK MICHAL; ABBASI AMIR REZA; Ebrahimzadeh Mohammad Esmaeil; Babaei Fateme; Khanpour Matikolaei Mojtaba

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Journal: JOURNAL OF NANOSTRUCTURES Year:2019 | Volume:9 | Issue:1 Page(s): 8-13

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Title

Synthesis and Crystal Structure of [Pb(gly)2]n; New lead(II) Coordination Polymer with Glycine Ligand

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Keywords

Coordination Polymer

Glycine

Lead(II) Oxide

Nano Particle

Abstract

[Pb(gly)2]n (1) (gly is the abbreviation of Glycine) have been synthesized and characterized by elemental analyses, IR, 1 H NMR and 13 C NMR spectroscopy. The single crystal structure of 1 show the complex is 2D Coordination Polymer with octahedral environment that is formed into 3D supramolecule through hydrogen bond. Structural determination of compound 1 reveals the Pb(II) ion is four coordinated, bonded to a nitrogen, oxygen and two carbon atoms from the Glycine ligand. PbO nanoparticles were synthesized by calcinations of compound 1 at 500, 550 and 600 ° C under air atmosphere. The PbO nanostructure was characterized by scanning electron microscopy (SEM) and X-ray powder diffraction (XRD). The thermal stability of compound 1 was studied by thermal gravimetric (TG) and differential thermal analyses (DTA).

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APA: Copy

shokhchashm, Zarnoosh, Hakimifar, Azar, HASHEMI, LIDA, MORSALI, ALI, DUSEK, MICHAL, ABBASI, AMIR REZA, Ebrahimzadeh, Mohammad Esmaeil, Babaei, Fateme, & Khanpour Matikolaei, Mojtaba. (2019). Synthesis and Crystal Structure of [Pb(gly)2]n; New lead(II) Coordination Polymer with Glycine Ligand. JOURNAL OF NANOSTRUCTURES, 9(1), 8-13. SID. https://sid.ir/paper/744896/en

Vancouver: Copy

shokhchashm Zarnoosh, Hakimifar Azar, HASHEMI LIDA, MORSALI ALI, DUSEK MICHAL, ABBASI AMIR REZA, Ebrahimzadeh Mohammad Esmaeil, Babaei Fateme, Khanpour Matikolaei Mojtaba. Synthesis and Crystal Structure of [Pb(gly)2]n; New lead(II) Coordination Polymer with Glycine Ligand. JOURNAL OF NANOSTRUCTURES[Internet]. 2019;9(1):8-13. Available from: https://sid.ir/paper/744896/en

IEEE: Copy

Zarnoosh shokhchashm, Azar Hakimifar, LIDA HASHEMI, ALI MORSALI, MICHAL DUSEK, AMIR REZA ABBASI, Mohammad Esmaeil Ebrahimzadeh, Fateme Babaei, and Mojtaba Khanpour Matikolaei, “Synthesis and Crystal Structure of [Pb(gly)2]n; New lead(II) Coordination Polymer with Glycine Ligand,” JOURNAL OF NANOSTRUCTURES, vol. 9, no. 1, pp. 8–13, 2019, [Online]. Available: https://sid.ir/paper/744896/en

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