Molecular Dynamics, Biological Study and Extractive Spectrophotometric Determination of Vanadium (V)-2-methyl-8-quinolinol Complex

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Shiwani Singh; Agnithotri Nivedita; Rathi Parveen; Agnithotri Rajesh; KUMAR VIKAS

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Journal: Iranian Journal of Chemistry and Chemical Engineering Year:2021 | Volume:40 | Issue:1 Page(s): 207-214

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Title

Molecular Dynamics, Biological Study and Extractive Spectrophotometric Determination of Vanadium (V)-2-methyl-8-quinolinol Complex

Author(s)

Keywords

Vanadium (V)

2-methyl-8-quinolinol

Extraction

Spectrophotometric determination

Structural elucidation

Antimicrobial activity

Abstract

An extractive spectrophotometric method is developed for the trace determination of vanadium (V). 2-methyl-8-quinolinol(MQ) reacts with vanadium(V) to form a 1: 2 (V: MQ) light brown complex in an aqueous medium at 0. 05 M CH3COOH concentration which is quantitatively extractable into chloroform exhibiting maximum absorbance in the range 397-405 nm. . The complex is synthesized in 1: 2 ratio and the structure of the formed complex is elucidated on the basis of IR, NMR, and TGA techniques aided with computational studies. The formed V (V)-MQ complex is also screened for its in vitro Antimicrobial activity. The method obeys Beer’ s law up to 6. 2 μ g V/mL with molar absorptivity and Sandell’ s sensitivity of 2. 449 × 103 L/mol. cm and 0. 0208 μ g V/cm2, respectively, at 400 nm. The method is simple, rapid, and has good reproducibility with a standard deviation of ± 0. 0027 absorbance units.

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APA: Copy

Shiwani, Singh, Agnithotri, Nivedita, Rathi, Parveen, Agnithotri, Rajesh, & KUMAR, VIKAS. (2021). Molecular Dynamics, Biological Study and Extractive Spectrophotometric Determination of Vanadium (V)-2-methyl-8-quinolinol Complex. IRANIAN JOURNAL OF CHEMISTRY AND CHEMICAL ENGINEERING (IJCCE), 40(1), 207-214. SID. https://sid.ir/paper/776299/en

Vancouver: Copy

Shiwani Singh, Agnithotri Nivedita, Rathi Parveen, Agnithotri Rajesh, KUMAR VIKAS. Molecular Dynamics, Biological Study and Extractive Spectrophotometric Determination of Vanadium (V)-2-methyl-8-quinolinol Complex. IRANIAN JOURNAL OF CHEMISTRY AND CHEMICAL ENGINEERING (IJCCE)[Internet]. 2021;40(1):207-214. Available from: https://sid.ir/paper/776299/en

IEEE: Copy

Singh Shiwani, Nivedita Agnithotri, Parveen Rathi, Rajesh Agnithotri, and VIKAS KUMAR, “Molecular Dynamics, Biological Study and Extractive Spectrophotometric Determination of Vanadium (V)-2-methyl-8-quinolinol Complex,” IRANIAN JOURNAL OF CHEMISTRY AND CHEMICAL ENGINEERING (IJCCE), vol. 40, no. 1, pp. 207–214, 2021, [Online]. Available: https://sid.ir/paper/776299/en

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