BICYCLIC AZIRIDINE-BASED ELECTROCHEMICAL TRAMADOL NANOSENSOR

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KHOSHCHINGOL S.; MAHMOODI N.O.; ISLAMNEZHAD A.

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Seminar Paper

Paper Information

Seminar: IRANIAN BIENNIAL ELECTROCHEMISTRY SEMINAR
Year:2014 | Issue:11

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Title

BICYCLIC AZIRIDINE-BASED ELECTROCHEMICAL TRAMADOL NANOSENSOR

Author(s)

KHOSHCHINGOL S. | MAHMOODI N.O. | ISLAMNEZHAD A. | Issue Writer Certificate

Keywords

TRAMADOL

BICYCLIC AZIRIDINE

DIFFERENTIAL PULSE VOLTAMMETRY

NANOGRAPHENE

Abstract

TRAMADOL (TRA) IS A CENTRALLY ACTING ANALGESIC THAT WAS FIRST INTRODUCED IN GERMANY IN 1977. TODAY, IT HAS BECOME THE MOST PRESCRIBED OPIOID WORLDWIDE. IT IS GENERALLY SAID TO BE DEVOID OF MANY OF THE SERIOUS ADVERSE EFFECTS OF TRADITIONAL OPIOID RECEPTOR AGONISTS SUCH AS THE RISK FOR RESPIRATORY DEPRESSION AND DRUG DEPENDENCE. TRAMADOL WORKS IN TWO WAYS TO RELIEVE PAIN. IT WORKS ON THE BRAIN IN A SIMILAR WAY TO CODEINE AND MORPHINE. IT ALSO AFFECTS SOME OTHER CHEMICALS IN THE BRAIN CALLED NORADRENALINE AND SEROTONIN. THESE HAVE MANY FUNCTIONS, SOME OF WHICH INCLUDE EASING PAIN [1-2]. A VARIETY OF QUANTITATIVE ANALYTICAL METHODS HAVE BEEN REPORTED FOR THE DETERMINATION OF TRA INCLUDING HPLC, LC-MS AND GC-MS. ELECTROCHEMICAL ANALYTIC TECHNIQUE IS AN ATTRACTIVE METHODDUE TO SIMPLICITY, RAPIDITY, LOW EXPENSE, HIGH SENSITIVITY AND POSSIBILITY OFMINIATURIZATION. CONSTRUCTION OF ELECTROCHEMICAL SENSORS CONTINUES TO BE AN AREA OF GREAT INTEREST [3]. THE ELECTROCHEMICAL BEHAVIOR OF TRAIN AQUEOUS MEDIA HAS BEEN EXAMINED BY CYCLIC AND DIFFERENTIAL PULSE VOLTAMMETRY. THE VOLTAMMOGRAMS WERE RECORDED WITH MAUTOLAB FRA2 POTENTIOSTAT-GALVANOSTAT. A THREE-ELECTRODE SYSTEM WAS USED WITH A BICYCLOAZIRIDIN-NANOGRAPHENE MODIFIED ELECTRODE AS WORKING, A PLATINUM ROD AS THE COUNTER ELECTRODE AND AN AG/AGCL AS THE REFERENCE ELECTRODE. ALL TESTS WERE CARRIED OUT UNDER ROOM TEMPERATURE AND N2 ATMOSPHERE. THE PH STRONGLY AFFECTS THE PEAK POTENTIAL OF TRA. THE BEST ANALYTICAL RESPONSE WAS OBTAINED AT PH 9.0. THE CATHODIC PEAK CURRENTS WERE PROPORTIONAL TO TRA CONCENTRATIONS. THE EFFECT OF POTENTIAL SCAN RATE ON THE PEAK POTENTIAL AND PEAK CURRENT OF TRA WAS INVESTIGATED. THE CORRELATION OF THE PEAK CURRENTS AGAINST V1/2 (V IS THE SCAN RATE) IS LINEAR, WHICH IS VERY SIMILAR TO A DIFFUSION-CONTROLLED PROCESS. PROPOSED METHOD APPLIED TO ANALYSIS OF COMMERCIAL TABLETS, SUCCESSFULLY.

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APA: Copy

KHOSHCHINGOL, S., MAHMOODI, N.O., & ISLAMNEZHAD, A.. (2014). BICYCLIC AZIRIDINE-BASED ELECTROCHEMICAL TRAMADOL NANOSENSOR. IRANIAN BIENNIAL ELECTROCHEMISTRY SEMINAR. SID. https://sid.ir/paper/909295/en

Vancouver: Copy

KHOSHCHINGOL S., MAHMOODI N.O., ISLAMNEZHAD A.. BICYCLIC AZIRIDINE-BASED ELECTROCHEMICAL TRAMADOL NANOSENSOR. 2014. Available from: https://sid.ir/paper/909295/en

IEEE: Copy

S. KHOSHCHINGOL, N.O. MAHMOODI, and A. ISLAMNEZHAD, “BICYCLIC AZIRIDINE-BASED ELECTROCHEMICAL TRAMADOL NANOSENSOR,” presented at the IRANIAN BIENNIAL ELECTROCHEMISTRY SEMINAR. 2014, [Online]. Available: https://sid.ir/paper/909295/en

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