SYNTHESIS OF 1, 1' - BIS [4- (DIMETHYLSILYL) BUTYL] FERROCENE VIA A GRIGNARD REACTION

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TEIMURI MOFRAD R.; RAHIMPOUR K.

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Seminar Paper

Paper Information

Seminar: IRANIAN SEMINAR OF ORGANIC CHEMISTRY
Year:2014 | Issue:22

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Title

SYNTHESIS OF 1, 1' - BIS [4- (DIMETHYLSILYL) BUTYL] FERROCENE VIA A GRIGNARD REACTION

Author(s)

TEIMURI MOFRAD R. | RAHIMPOUR K. | Issue Writer Certificate

Keywords

FERROCENE

SILANE

GRIGNARD REACTION

Abstract

FERROCENE AND ITS DERIVATIVES HAVE BEEN EMPLOYED FOR A VERY LONG TIME AS COMBUSTION CATALYSTS IN PROPELLANT COMPOSITIONS. IT HAS BEEN FOUND THAT THEIR PROPERTIES ARE IMPROVED BY THE ADDITION OF ORGANOSILYL RADICALS BOUND DIRECTLY BY CARBON-SILICON BONDS TO THE CYCLOPENTADIENYL NUCLEUS OF THE FERROCENE. SUCH COMPOUNDS ARE SYNTHESIZED FROM VARIOUS SYNTHETICROUTES, THAT THE MOST IMPORTANT OF THEM IS THE GRIGNARD REACTION [1].2TORGANOSILICON REAGENTS AND COMPOUNDS ARE VALUABLE IN ORGANICSYNTHESIS, SO METHODS TO SYNTHESIZE THEM HAVE BECOME OF CONSIDERABLE IMPORTANCE [2, 3].WE REPORT HERE SYNTHESIS OF 2T1, 1' - BIS [4- (DIMETHYLSILYL) BUTYL] FERROCENE BY A 2TGRIGNARD REACTION FROM1, 1' -BIS (4-CHLOROBUTYL) FERROCENE IN THF.1, 1' -BIS (4-CHLOROBUTYL) FERROCENE WAS PREPARED BY FRIEDEL-CRAFTS ACYLATIONOF FERROCENE WITH 4-CHLOROBUTYROYL CHLORIDE IN DICHLOROMETHANE INTHE PRESENCE OF ALCL3 AS CATALYST. 1, 1' -BIS (4-CHLOROBUTYROYL) FERROCENE WAS REDUCED TO 1, 1' -BIS (4-CHLOROBUTYL) FERROCENEBY NABH4 IN DIGLYME.

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APA: Copy

TEIMURI MOFRAD, R., & RAHIMPOUR, K.. (2014). SYNTHESIS OF 1, 1' - BIS [4- (DIMETHYLSILYL) BUTYL] FERROCENE VIA A GRIGNARD REACTION. IRANIAN SEMINAR OF ORGANIC CHEMISTRY. SID. https://sid.ir/paper/912620/en

Vancouver: Copy

TEIMURI MOFRAD R., RAHIMPOUR K.. SYNTHESIS OF 1, 1' - BIS [4- (DIMETHYLSILYL) BUTYL] FERROCENE VIA A GRIGNARD REACTION. 2014. Available from: https://sid.ir/paper/912620/en

IEEE: Copy

R. TEIMURI MOFRAD, and K. RAHIMPOUR, “SYNTHESIS OF 1, 1' - BIS [4- (DIMETHYLSILYL) BUTYL] FERROCENE VIA A GRIGNARD REACTION,” presented at the IRANIAN SEMINAR OF ORGANIC CHEMISTRY. 2014, [Online]. Available: https://sid.ir/paper/912620/en

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