PREPARATION OFPOLY (METHYL METHACRYLATE) -BASEDNANOCOMPOSITE BY RAFT POLYMERIZATION

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GHAFFARI GHALEH MAHNAZ; RASHIDZADEH BAHAEDIN; HOSSEINZADEH HOSSEIN

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Seminar Paper

Paper Information

Seminar: IRANIAN SEMINAR OF ORGANIC CHEMISTRY
Year:2014 | Issue:22

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Title

PREPARATION OFPOLY (METHYL METHACRYLATE) -BASEDNANOCOMPOSITE BY RAFT POLYMERIZATION

Author(s)

GHAFFARI GHALEH MAHNAZ | RASHIDZADEH BAHAEDIN | HOSSEINZADEH HOSSEIN | Issue Writer Certificate

Keywords

NANOCOMPOSITE

METHYL METHACRYLATE

RAFTPOLYMERIZATION

SIO2

Abstract

LIVING CONTROLLED RADICAL POLYMERIZATION HAS BEEN A POWERFUL TECHNIQUE TOSYNTHESIZE WELL-DEFINED STRUCTURE POLYMER BY CONTROLLING MOLECULAR WEIGHT, MOLECULAR WEIGHT DISTRIBUTION AND TAILORED ARCHITECTURE. THREE ‘‘LIVING’’ RADICALPOLYMERIZATION TECHNIQUES WHICH ARE RECEIVING MORE AND MORE ATTENTION INACADEMIA ARE NITROXIDE-MEDIATED RADICAL POLYMERIZATION (NMP) [1], ATOM TRANSFERRADICAL POLYMERIZATION (ATRP) [2], AND REVERSIBLE ADDITION–FRAGMENTATION CHAINTRANSFER (RAFT) POLYMERIZATION [3]. RAFT POLYMERIZATION WAS CONSIDERED AS ONE OFTHE MOST PROMISING CONTROLLED FREE RADICAL POLYMERIZATION DUE TO ITS COMPATIBILITYWITH A WIDE RANGE OF MONOMERS AND ITS VERSATILITY.IN THE PRESENT WORK, A NOVEL NANOCOMPOSITE WAS PREPARED BASED ON POLY (METHYL METHACRYLATE) /SIO2 USING 4-CYANO-4- [(PHENYLCARBOTHIOYL) SULFANYL] PENTANOIC ACID AS A RAFT AGENT (FIGURE 1).THE STRUCTURE, MORPHOLOGY AND THERMAL PROPERTIES OF THE NANOCOMPOSITES WERE CHARACTERIZED USING FOURIER TRANSFORM INFRARED (FT-IR), HNMR, TRANSMISSION ELECTRON MICROSCOPY (TEM), THERMOGRAVIMETRIC ANALYSIS (TGA), AND DIFFERENTIAL SCANNING CALORIMETRY (DSC), RESPECTIVELY. THE XRD RESULTS ALSO SHOWED THE PROPER INTERCALATION OF POLYMER CHAINS BETWEEN THE SILICATE LAYERS.

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APA: Copy

GHAFFARI GHALEH, MAHNAZ, RASHIDZADEH, BAHAEDIN, & HOSSEINZADEH, HOSSEIN. (2014). PREPARATION OFPOLY (METHYL METHACRYLATE) -BASEDNANOCOMPOSITE BY RAFT POLYMERIZATION. IRANIAN SEMINAR OF ORGANIC CHEMISTRY. SID. https://sid.ir/paper/912989/en

Vancouver: Copy

GHAFFARI GHALEH MAHNAZ, RASHIDZADEH BAHAEDIN, HOSSEINZADEH HOSSEIN. PREPARATION OFPOLY (METHYL METHACRYLATE) -BASEDNANOCOMPOSITE BY RAFT POLYMERIZATION. 2014. Available from: https://sid.ir/paper/912989/en

IEEE: Copy

MAHNAZ GHAFFARI GHALEH, BAHAEDIN RASHIDZADEH, and HOSSEIN HOSSEINZADEH, “PREPARATION OFPOLY (METHYL METHACRYLATE) -BASEDNANOCOMPOSITE BY RAFT POLYMERIZATION,” presented at the IRANIAN SEMINAR OF ORGANIC CHEMISTRY. 2014, [Online]. Available: https://sid.ir/paper/912989/en

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