PREPARATION OF IRON BASED CATALYSTS VIA SIMPLE PYROLYSIS METHOD FOR HIGH TEMPERATURE WATER GAS SHIFT REACTION

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MESHKANI F.; REZAEI M.

مرکز اطلاعات علمی Scientific Information Database (SID) - Trusted Source for Research and Academic Resources

Seminar Paper

Paper Information

Seminar: CHEMICAL ENGINEERING CONGRESS AND EXHIBITION
Year:2014 | Issue:8

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Title

PREPARATION OF IRON BASED CATALYSTS VIA SIMPLE PYROLYSIS METHOD FOR HIGH TEMPERATURE WATER GAS SHIFT REACTION

Author(s)

MESHKANI F. | REZAEI M. | Issue Writer Certificate

Keywords

PYROLYSIS

ETHYLENE GLYCOL

IRON BASED CATALYST

NANOCRYSTALLINE

WATER-GAS SHIFT

Abstract

NANOCRYSTALLINE FE3O4 BASED CATALYSTS WERE SYNTHESIZED BY A FACILE DIRECT PYROLYSIS OF FERRIC NITRATE (ETHYLENE GLYCOL) GEL IN THE AIR ATMOSPHERE WITHOUT ADDING ANY TEMPLATE AND SURFACTANT AND EMPLOYED IN HIGH TEMPERATURE WATER GAS SHIFT REACTION. THE PREPARED CATALYSTS WERE CHARACTERIZED BY POWDER X-RAY DIFFRACTION (XRD), N2 ADSORPTION (BET), TEMPERATURE PROGRAMMED REDUCTION (TPR) TECHNIQUES. XRD ANALYSIS SHOWED THAT THIS METHOD LED TO OBTAINING THE CATALYSTS DIRECTLY IN THE ACTIVE PHASE WITH CHROMIUM AND COPPER INCORPORATED INTO MAGNETITE LATTICE. THE RESULTS SHOWED THAT THE ADDITION OF CHROMIUM SIGNIFICANTLY INCREASES THE BET SURFACE AREA AND PORE VOLUME OF THE PURE IRON OXIDE. AMONG THE CATALYSTS EVALUATED, FE-CR-CU CATALYST REVEALED HIGHER CATALYTIC PERFORMANCE COMPARED TO COMMERCIAL CATALYST. IN ADDITION, THE EFFECT OF STEAM TO GAS RATIO AND GHSV ON THE CATALYTIC PERFORMANCE OF THE CATALYST WITH HIGHEST ACTIVITY HAS BEEN ALSO STUDIED.

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APA: Copy

MESHKANI, F., & REZAEI, M.. (2014). PREPARATION OF IRON BASED CATALYSTS VIA SIMPLE PYROLYSIS METHOD FOR HIGH TEMPERATURE WATER GAS SHIFT REACTION. INTERNATIONAL CHEMICAL ENGINEERING CONGRESS AND EXHIBITION. SID. https://sid.ir/paper/916612/en

Vancouver: Copy

MESHKANI F., REZAEI M.. PREPARATION OF IRON BASED CATALYSTS VIA SIMPLE PYROLYSIS METHOD FOR HIGH TEMPERATURE WATER GAS SHIFT REACTION. 2014. Available from: https://sid.ir/paper/916612/en

IEEE: Copy

F. MESHKANI, and M. REZAEI, “PREPARATION OF IRON BASED CATALYSTS VIA SIMPLE PYROLYSIS METHOD FOR HIGH TEMPERATURE WATER GAS SHIFT REACTION,” presented at the INTERNATIONAL CHEMICAL ENGINEERING CONGRESS AND EXHIBITION. 2014, [Online]. Available: https://sid.ir/paper/916612/en

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