Development of a Green Single Drop Microextraction Based on Deep Eutectic Solvent and HPLC-UV for Trace Residue Analysis of Three Frequent-Used Pesticides

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POURHOSSEIN MEHRAN; KHADEM MONIREH; OMIDI FARIBORZ; Heravizadeh Omid Reza; SHAHTAHERI SEYED JAMALEDDIN

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Journal Paper

Paper Information

Journal: Iranian Journal of Public Health Year:2023 | Volume:52 | Issue:11 Page(s): 2440-2449

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Title

Development of a Green Single Drop Microextraction Based on Deep Eutectic Solvent and HPLC-UV for Trace Residue Analysis of Three Frequent-Used Pesticides

Author(s)

Keywords

Single drop microextraction

Metribuzin

Dichlorvos

Fenthion

Abstract

Background: A green sample preparation method named deep eutectic solvent-based Single drop microextraction (DES-SDME) was developed and optimized for determining trace Metribuzin, Dichlorvos, and Fenthion. Methods: Two hundred seventy experimental runs were performed, and the optimal values of the five influential factors in the DES-SDME method were determined. The design of the study was based on one factor at a time and the peak area of high-performance liquid chromatography was used as a benchmark for comparing analysis results. Results: After optimizing the effective factors, the linearity range, detection limit and quantification limit of the method were determined by drawing calibration curves for the studied analytes. Conclusion: The results indicated the success of the developed method in obtaining acceptable figures of merit as a green preparation method with accuracy and precision.

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APA: Copy

POURHOSSEIN, MEHRAN, KHADEM, MONIREH, OMIDI, FARIBORZ, Heravizadeh, Omid Reza, & SHAHTAHERI, SEYED JAMALEDDIN. (2023). Development of a Green Single Drop Microextraction Based on Deep Eutectic Solvent and HPLC-UV for Trace Residue Analysis of Three Frequent-Used Pesticides. IRANIAN JOURNAL OF PUBLIC HEALTH, 52(11), 2440-2449. SID. https://sid.ir/paper/1101145/en

Vancouver: Copy

POURHOSSEIN MEHRAN, KHADEM MONIREH, OMIDI FARIBORZ, Heravizadeh Omid Reza, SHAHTAHERI SEYED JAMALEDDIN. Development of a Green Single Drop Microextraction Based on Deep Eutectic Solvent and HPLC-UV for Trace Residue Analysis of Three Frequent-Used Pesticides. IRANIAN JOURNAL OF PUBLIC HEALTH[Internet]. 2023;52(11):2440-2449. Available from: https://sid.ir/paper/1101145/en

IEEE: Copy

MEHRAN POURHOSSEIN, MONIREH KHADEM, FARIBORZ OMIDI, Omid Reza Heravizadeh, and SEYED JAMALEDDIN SHAHTAHERI, “Development of a Green Single Drop Microextraction Based on Deep Eutectic Solvent and HPLC-UV for Trace Residue Analysis of Three Frequent-Used Pesticides,” IRANIAN JOURNAL OF PUBLIC HEALTH, vol. 52, no. 11, pp. 2440–2449, 2023, [Online]. Available: https://sid.ir/paper/1101145/en

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