COMPARISON OF HEAD SPACE SOLID PHASE MICROEXTRACTION (HSSPME) AND HYDRO-DISTILLATION (HD) TECHNIQUES IN DETERMINATION OF ESSENTIAL OILS IN FRITILLARIA IMPERIALIS

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SEYED SALEH S.S.; ARABI S.; ASHOURI F.

مرکز اطلاعات علمی Scientific Information Database (SID) - Trusted Source for Research and Academic Resources

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Journal: Journal of Medicinal Plants Year:2018 | Volume:17 | Issue:68 Page(s): 122-135

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Title

COMPARISON OF HEAD SPACE SOLID PHASE MICROEXTRACTION (HSSPME) AND HYDRO-DISTILLATION (HD) TECHNIQUES IN DETERMINATION OF ESSENTIAL OILS IN FRITILLARIA IMPERIALIS

Author(s)

SEYED SALEH S.S. | ARABI S. | ASHOURI F. | Issue Writer Certificate

Keywords

FRITILLARIA IMPERIALISQ1

GC-MSQ2

HEAD SPACE SOLID PHASE MICROEXTRACTION (HS-SPME)Q1

HYDRODISTILLATION (HD)Q1

Abstract

Background: FRITILLARIA IMPERIALIS is an endangered species with pharmaceutical alkaloids that can be effective in reducing blood pressure and reducing cardiac palpitations.Objective: Comparison of head space solid phase microextraction (HS-SPME) and hydrodistillation (HD) techniques in determination of essential oils in FRITILLARIA IMPERIALIS Methods: Quality and quantity determination of components of extracted essential oils from aerial parts of FRITILLARIA IMPERIALIS by Head space-Solid phase microextraction (HS-SPME) and hydro-distillation (HD) techniques using Gas Chromatography-Mass Spctroscopy (GC-MS) method.Results: 24 components (86.61%) were identified in the oil was isolated by hydrodistillation.The major components of oil of F.imperialis were a-Bisabolol oxide A (28.2%), Camphor (12.86%), Chamazulene (11.8%), Trans-Thujone (10.9%), a-Bisabolone oxide A (10.3%), d-3-Carene (6.9%) and a-Pinene (5.65%).21 components (94.93%) were characterized in the oil which was obtained by Head space-solid phase microextraction (HS-SPME). The major components of the oil were a-Bisabolol oxide A (35.2%), Camphor (9.54%), Chamazulene (18.3%), Trans-Thujone (7.89%), a-Bisabolone oxide A (11.8%), d-3-Carene (6.5%) and a-Pinene (5.7%).Conclusion: In both methods (HD & HS-SPME), oxygenated sesquiterpenes were the main components of the oil, whereas hydrocarbon sesquiterpens were trace.

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APA: Copy

SEYED SALEH, S.S., ARABI, S., & ASHOURI, F.. (2018). COMPARISON OF HEAD SPACE SOLID PHASE MICROEXTRACTION (HSSPME) AND HYDRO-DISTILLATION (HD) TECHNIQUES IN DETERMINATION OF ESSENTIAL OILS IN FRITILLARIA IMPERIALIS. JOURNAL OF MEDICINAL PLANTS, 17(68 ), 122-135. SID. https://sid.ir/paper/15278/en

Vancouver: Copy

SEYED SALEH S.S., ARABI S., ASHOURI F.. COMPARISON OF HEAD SPACE SOLID PHASE MICROEXTRACTION (HSSPME) AND HYDRO-DISTILLATION (HD) TECHNIQUES IN DETERMINATION OF ESSENTIAL OILS IN FRITILLARIA IMPERIALIS. JOURNAL OF MEDICINAL PLANTS[Internet]. 2018;17(68 ):122-135. Available from: https://sid.ir/paper/15278/en

IEEE: Copy

S.S. SEYED SALEH, S. ARABI, and F. ASHOURI, “COMPARISON OF HEAD SPACE SOLID PHASE MICROEXTRACTION (HSSPME) AND HYDRO-DISTILLATION (HD) TECHNIQUES IN DETERMINATION OF ESSENTIAL OILS IN FRITILLARIA IMPERIALIS,” JOURNAL OF MEDICINAL PLANTS, vol. 17, no. 68 , pp. 122–135, 2018, [Online]. Available: https://sid.ir/paper/15278/en

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