DETERMINATION OF CARBAMAZEPINE IN BIOLOGICAL SAMPLES USING ULTRASOUND-ASSISTED EMULSIFICATION MICRO-EXTRACTION AND GAS CHROMATOGRAPHY

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BAHMAEI MANOOCHEHR; KHALILIAN FAEZEH; MASHAYEKHI HOSSEIN ALI

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Journal Paper

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Journal: Journal of Chemical Health Risks Year:2015 | Volume:5 | Issue:1 Page(s): 55-65

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Title

DETERMINATION OF CARBAMAZEPINE IN BIOLOGICAL SAMPLES USING ULTRASOUND-ASSISTED EMULSIFICATION MICRO-EXTRACTION AND GAS CHROMATOGRAPHY

Author(s)

BAHMAEI MANOOCHEHR | KHALILIAN FAEZEH | MASHAYEKHI HOSSEIN ALI | Issue Writer Certificate

Keywords

ULTRASOUND-ASSISTED

EMULSIFICATION

MICROEXTRACTION

CARBAMAZEPINE

GAS CHROMATOGRAPHY

BIOLOGICAL SAMPLES

Abstract

In this study, simple and efficient ULTRASOUND-ASSISTED EMULSIFICATION MICROEXTRACTION (USAEME) combined with GAS CHROMATOGRAPHY-flame ionization detector (GCFID) was developed for the preconcentration and determination of CARBAMAZEPINE in BIOLOGICAL SAMPLES. In this method, the fine droplets of 1-octanol were formed and dispersed in the sample with the help of ultrasonic waves, which accelerated the formation of the fine cloudy solution without using disperser solvents. Several factors influencing the extraction efficiency such as the nature and volume of organic solvent, extraction temperature, ionic strength and centrifugation time were investigated and optimized. The new method (USAEME) provided detection limits of 0.6 mg L-1 and 1.2 mg L-1 in urine and plasma samples, respectively. The calibration graphs were linear in the range of 2.5-500 mg L-1 and 5.0-500 mg L-1 in urine and plasma, respectively. This proposed method was successfully applied to the analysis of CARBAMAZEPINE in BIOLOGICAL SAMPLES.

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APA: Copy

BAHMAEI, MANOOCHEHR, KHALILIAN, FAEZEH, & MASHAYEKHI, HOSSEIN ALI. (2015). DETERMINATION OF CARBAMAZEPINE IN BIOLOGICAL SAMPLES USING ULTRASOUND-ASSISTED EMULSIFICATION MICRO-EXTRACTION AND GAS CHROMATOGRAPHY. JOURNAL OF CHEMICAL HEALTH RISKS (JCHR), 5(1), 55-65. SID. https://sid.ir/paper/340257/en

Vancouver: Copy

BAHMAEI MANOOCHEHR, KHALILIAN FAEZEH, MASHAYEKHI HOSSEIN ALI. DETERMINATION OF CARBAMAZEPINE IN BIOLOGICAL SAMPLES USING ULTRASOUND-ASSISTED EMULSIFICATION MICRO-EXTRACTION AND GAS CHROMATOGRAPHY. JOURNAL OF CHEMICAL HEALTH RISKS (JCHR)[Internet]. 2015;5(1):55-65. Available from: https://sid.ir/paper/340257/en

IEEE: Copy

MANOOCHEHR BAHMAEI, FAEZEH KHALILIAN, and HOSSEIN ALI MASHAYEKHI, “DETERMINATION OF CARBAMAZEPINE IN BIOLOGICAL SAMPLES USING ULTRASOUND-ASSISTED EMULSIFICATION MICRO-EXTRACTION AND GAS CHROMATOGRAPHY,” JOURNAL OF CHEMICAL HEALTH RISKS (JCHR), vol. 5, no. 1, pp. 55–65, 2015, [Online]. Available: https://sid.ir/paper/340257/en

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