POLYSTYRENE SUPPORTED [N-(ALANINE) SULFONAMIDE]/PALLADIUM CHLORIDE: SYNTHESIS, CHARACTERIZATION, FOR HECK COUPLING REACTIONS

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SHAFIEYOON P.; MEHDIPOUR E.

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Journal: ORGANIC CHEMISTRY RESEARCH Year:2018 | Volume:4 | Issue:1 Page(s): 100-109

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Title

POLYSTYRENE SUPPORTED [N-(ALANINE) SULFONAMIDE]/PALLADIUM CHLORIDE: SYNTHESIS, CHARACTERIZATION, FOR HECK COUPLING REACTIONS

Author(s)

SHAFIEYOON P. | MEHDIPOUR E. | Issue Writer Certificate

Keywords

[N- (ALANINE)] PARA -STYRENE SULFONAMIDE

POLYSTYRENE [N- (ALANINE) SULFONAMIDE]

POLY STYRENE [N- (ALANINE) SULFONAMIDE] / PALLADIUM CHLORIDE

POLYMER-SUPPORTED PALLADIUM

HECK REACTION

Abstract

para-styrene sulfonyl chloride and (S) - (+) -alanine in the presence of KOH 1 M as a base, and CHCl3 was used as solvent. The formation/presence of monomer was verified using FT-IR and 1H NMR spectroscopy. Polystyrene [N- (alanine) sulfonamide] (PASS) was also prepared from the polymerization of [N- (alanine)] para-styrene sulfonamide (ASS) in the presence of AIBN (azoisobutyronitrile) under atmosphere of nitrogen. Polystyrene [N- (alanine) sulfonamide] /palladium chloride as a polymer-supported palladium complex was also prepared from the reaction of PdCl2 (CH3CN) 2 with PASS in the presence of KOH 1 M. A green solid was consequently appeared. This catalyst was synthesized for the first time as a polymer-supported palladium and applied in Heck reactions.

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APA: Copy

SHAFIEYOON, P., & MEHDIPOUR, E.. (2018). POLYSTYRENE SUPPORTED [N-(ALANINE) SULFONAMIDE]/PALLADIUM CHLORIDE: SYNTHESIS, CHARACTERIZATION, FOR HECK COUPLING REACTIONS. ORGANIC CHEMISTRY RESEARCH, 4(1), 100-109. SID. https://sid.ir/paper/351222/en

Vancouver: Copy

SHAFIEYOON P., MEHDIPOUR E.. POLYSTYRENE SUPPORTED [N-(ALANINE) SULFONAMIDE]/PALLADIUM CHLORIDE: SYNTHESIS, CHARACTERIZATION, FOR HECK COUPLING REACTIONS. ORGANIC CHEMISTRY RESEARCH[Internet]. 2018;4(1):100-109. Available from: https://sid.ir/paper/351222/en

IEEE: Copy

P. SHAFIEYOON, and E. MEHDIPOUR, “POLYSTYRENE SUPPORTED [N-(ALANINE) SULFONAMIDE]/PALLADIUM CHLORIDE: SYNTHESIS, CHARACTERIZATION, FOR HECK COUPLING REACTIONS,” ORGANIC CHEMISTRY RESEARCH, vol. 4, no. 1, pp. 100–109, 2018, [Online]. Available: https://sid.ir/paper/351222/en

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