SYNTHESIS AND CRYSTAL STRUCTURE ANALYSES OF BIS[N(2-CHLORO-PHENYL) 4-NITRO- HIOBENZAMIDATO]MERCURY(II) COMPLEX

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HABIBI M.H.; TANGESTANINEZHAD S.; FALAH SHOJAEI A.

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Journal: Iranian Journal of Crystallography and Mineralogy Year:2005 | Volume:13 | Issue:1 Page(s): 19-28

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Title

SYNTHESIS AND CRYSTAL STRUCTURE ANALYSES OF BIS[N(2-CHLORO-PHENYL) 4-NITRO- HIOBENZAMIDATO]MERCURY(II) COMPLEX

Author(s)

HABIBI M.H. | TANGESTANINEZHAD S. | FALAH SHOJAEI A. | Issue Writer Certificate

Keywords

CRYSTAL STRUCTUREQ4

MERCURY(II) COMPLEXQ4

THIOBENZAMIDEQ3

Abstract

In this research N(2-chloro-phenyl)4-nitro-thiobenzamide as a ligand was synthesized. One mmol of mercury oxide was added to the solution of 1 mmol ligand in 45 ml chloroform and after 90 min the mixture through celite or BaS to remove unreacted mercury (II) compounds. The yellow crystals, which formed by slow evaporization, was separated and recrystallized from chloroform as fine yellow crystals with 87% yield and dried in vacuo. The CRYSTAL STRUCTURE of above complex was determined by single crystal X-ray diffraction method. The complex crystals in a monoclinic unit cell with a = 8.2822(9)A°, b = 12.2907(9) A°, c = 13.1243(13) A° a=90°, B = 98.729(5)°, g = 90° and Z = 2 and space group P21/c. The S-Hg-S is linear with angle of 180°.

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APA: Copy

HABIBI, M.H., TANGESTANINEZHAD, S., & FALAH SHOJAEI, A.. (2005). SYNTHESIS AND CRYSTAL STRUCTURE ANALYSES OF BIS[N(2-CHLORO-PHENYL) 4-NITRO- HIOBENZAMIDATO]MERCURY(II) COMPLEX. IRANIAN JOURNAL OF CRYSTALLOGRAPHY AND MINERALOGY, 13(1), 19-28. SID. https://sid.ir/paper/3779/en

Vancouver: Copy

HABIBI M.H., TANGESTANINEZHAD S., FALAH SHOJAEI A.. SYNTHESIS AND CRYSTAL STRUCTURE ANALYSES OF BIS[N(2-CHLORO-PHENYL) 4-NITRO- HIOBENZAMIDATO]MERCURY(II) COMPLEX. IRANIAN JOURNAL OF CRYSTALLOGRAPHY AND MINERALOGY[Internet]. 2005;13(1):19-28. Available from: https://sid.ir/paper/3779/en

IEEE: Copy

M.H. HABIBI, S. TANGESTANINEZHAD, and A. FALAH SHOJAEI, “SYNTHESIS AND CRYSTAL STRUCTURE ANALYSES OF BIS[N(2-CHLORO-PHENYL) 4-NITRO- HIOBENZAMIDATO]MERCURY(II) COMPLEX,” IRANIAN JOURNAL OF CRYSTALLOGRAPHY AND MINERALOGY, vol. 13, no. 1, pp. 19–28, 2005, [Online]. Available: https://sid.ir/paper/3779/en

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