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Information Journal Paper

Title

Effect of bias voltage on structure, morphology and hardness of ZrN coating deposited by reactive magnetron sputtering

Pages

  95-101

Abstract

 ZrN thin films were deposited on silicon (111) and 304 stainless steel substrates using direct current (DC) reactive magnetron sputtering. The effects of the substrate Bias voltage on the films’ structure, morphology, hardness were investigated. The films were characterized by X-ray diffraction (XRD), field emission scanning electron microscopy (FESEM), atomic force microscopy (AFM) and microhardness tester. XRD patterns showed grain size refinement from 19 to 13 nm with an increase of Bias voltage from 0 V to 150 V. In addition, (111) and (200) diffraction peaks were only present and other orientations were omitted. FESEM cross section of ZrN thin films showed a well aligned columnar structure. The increase of Bias voltage resulted in hardness rise to about 1720 Vickers at Bias voltage of 100 V. Negative Bias voltage induce an increase of the films density by the elimination of the porosity and voids. This maximum hardness can be interpreted by a maximum of the film density and minimum of the porosity

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    APA: Copy

    Madanypoor, Reza, Hasheminiasari, Masood, & Masoudpanah, Seyed Morteza. (2018). Effect of bias voltage on structure, morphology and hardness of ZrN coating deposited by reactive magnetron sputtering. METALLURGICAL ENGINEERING, 21(2 (70) ), 95-101. SID. https://sid.ir/paper/401916/en

    Vancouver: Copy

    Madanypoor Reza, Hasheminiasari Masood, Masoudpanah Seyed Morteza. Effect of bias voltage on structure, morphology and hardness of ZrN coating deposited by reactive magnetron sputtering. METALLURGICAL ENGINEERING[Internet]. 2018;21(2 (70) ):95-101. Available from: https://sid.ir/paper/401916/en

    IEEE: Copy

    Reza Madanypoor, Masood Hasheminiasari, and Seyed Morteza Masoudpanah, “Effect of bias voltage on structure, morphology and hardness of ZrN coating deposited by reactive magnetron sputtering,” METALLURGICAL ENGINEERING, vol. 21, no. 2 (70) , pp. 95–101, 2018, [Online]. Available: https://sid.ir/paper/401916/en

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